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Grapes - Thompson

doi:10.17617/3.7JFGDT

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Elena Levin

Volcani Institute, Agricultural Research Center

Dr. Itay Maoz group; Postharvest science department

Sample in glass vial

20ml

Solid-Phase Microextraction (SPME)

Sample details

Title Grapes - Thompson

Date of collection 2015-10-13

Collection method Sample in glass vial

Collection volume (of the vial) 20ml

Did not weight No

Mass of object sample 2g

Sample storage before sampling? No

Material state (old) Crushed

Salts Sodium chloride

Incubation duration 1sec

Incubation temperature 25°C

Sampling method

Sampling method Solid-Phase Microextraction (SPME)

Robotic automation Yes

What platform? Centri PAL3

Sorbent type DVB/Carbon-WR/PDMS

Sorbent phase thickness 80um

Headspace equilibrium temperature 40°C

Headspace equilibrium time 30min

Extraction mode Yes

Extraction time 30min

Extraction temperature 40°C

Desorption time 5min

Desorption temperature 250°C

Vortex No

GC-MS

Column type HP-5ms

Column flow 23.823ml/min

Pressure 5.3171psi

Length 30m

Inner diameter 250mm

Film thickness 0.25μm

Carrier gas He

Temperature ramps

Number of ramps 2

GC initial temperature 40°C

GC initial temperature hold time 1min

GC first temperature ramp rate 5°C/min

GC second temperature 160°C

GC second temperature hold time 2min

GC second temperature ramp rate 10°C/min

GC final temperature 250°C

GC final temperature hold time 1 min

Mass Spectrometer detectors Quadrupole-MS (Agilent)

Filament Voltage 1191V

Scan mass range 40-250

Data rate 50Hz

Ionisation -70eV

Grapes - Superior

doi:10.17617/3.TBE748

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Elena Levin

Volcani Institute, Agricultural Research Center

Dr. Itay Maoz group; Postharvest science department

Sample in glass vial

20ml

Solid-Phase Microextraction (SPME)

Sample details

Title Grapes - Superior

Date of collection 2015-08-27

Collection method Sample in glass vial

Collection volume (of the vial) 20ml

Did not weight No

Mass of object sample 2g

Sample storage before sampling? No

Material state (old) Crushed

Salts Sodium chloride

Incubation duration 1sec

Incubation temperature 25°C

Sampling method

Sampling method Solid-Phase Microextraction (SPME)

Robotic automation Yes

What platform? Centri PAL3

Sorbent type DVB/Carbon-WR/PDMS

Sorbent phase thickness 80um

Headspace equilibrium temperature 40°C

Headspace equilibrium time 30min

Extraction mode Yes

Extraction time 30min

Extraction temperature 40°C

Desorption time 5min

Desorption temperature 250°C

Vortex No

GC-MS

Column type HP-5ms

Column flow 23.823ml/min

Pressure 5.3171psi

Length 30m

Inner diameter 250mm

Film thickness 0.25μm

Carrier gas He

Temperature ramps

Number of ramps 2

GC initial temperature 40°C

GC initial temperature hold time 1min

GC first temperature ramp rate 5°C/min

GC second temperature 160°C

GC second temperature hold time 2min

GC second temperature ramp rate 10°C/min

GC final temperature 250°C

GC final temperature hold time 1 min

Mass Spectrometer detectors Quadrupole-MS (Agilent)

Filament Voltage 1191V

Scan mass range 40-250

Data rate 50Hz

Ionisation -70eV

Grapes - Sable seedless

doi:10.17617/3.APHKE6

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Elena Levin

Volcani Institute, Agricultural Research Center

Dr. Itay Maoz group; Postharvest science department

Sample in glass vial

20ml

Solid-Phase Microextraction (SPME)

Sample details

Title Grapes - Sable seedless

Date of collection 2015-08-25

Collection method Sample in glass vial

Collection volume (of the vial) 20ml

Did not weight No

Mass of object sample 2g

Sample storage before sampling? No

Material state (old) Crushed

Salts Sodium chloride

Incubation duration 1sec

Incubation temperature 25°C

Sampling method

Sampling method Solid-Phase Microextraction (SPME)

Robotic automation Yes

What platform? Centri PAL3

Sorbent type DVB/Carbon-WR/PDMS

Sorbent phase thickness 80um

Headspace equilibrium temperature 40°C

Headspace equilibrium time 30min

Extraction mode Yes

Extraction time 30min

Extraction temperature 40°C

Desorption time 5min

Desorption temperature 250°C

Vortex No

GC-MS

Column type HP-5ms

Column flow 23.823ml/min

Pressure 5.3171psi

Length 30m

Inner diameter 250mm

Film thickness 0.25μm

Carrier gas He

Temperature ramps

Number of ramps 2

GC initial temperature 40°C

GC initial temperature hold time 1min

GC first temperature ramp rate 5°C/min

GC second temperature 160°C

GC second temperature hold time 2min

GC second temperature ramp rate 10°C/min

GC final temperature 250°C

GC final temperature hold time 1 min

Mass Spectrometer detectors Quadrupole-MS (Agilent)

Filament Voltage 1191V

Scan mass range 40-250

Data rate 50Hz

Ionisation -70eV

Grapes - Quinerra

doi:10.17617/3.FKMMLK

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Elena Levin

Volcani Institute, Agricultural Research Center

Dr. Itay Maoz group; Postharvest science department

Sample in glass vial

20ml

Solid-Phase Microextraction (SPME)

Sample details

Title Grapes - Quinerra

Date of collection 2015-09-04

Collection method Sample in glass vial

Collection volume (of the vial) 20ml

Did not weight No

Mass of object sample 2g

Sample storage before sampling? No

Material state (old) Crushed

Salts Sodium chloride

Incubation duration 1sec

Incubation temperature 25°C

Sampling method

Sampling method Solid-Phase Microextraction (SPME)

Robotic automation Yes

What platform? Centri PAL3

Sorbent type DVB/Carbon-WR/PDMS

Sorbent phase thickness 80um

Headspace equilibrium temperature 40°C

Headspace equilibrium time 30min

Extraction mode Yes

Extraction time 30min

Extraction temperature 40°C

Desorption time 5min

Desorption temperature 250°C

Vortex No

GC-MS

Column type HP-5ms

Column flow 23.823ml/min

Pressure 5.3171psi

Length 30m

Inner diameter 250mm

Film thickness 0.25μm

Carrier gas He

Temperature ramps

Number of ramps 2

GC initial temperature 40°C

GC initial temperature hold time 1min

GC first temperature ramp rate 5°C/min

GC second temperature 160°C

GC second temperature hold time 2min

GC second temperature ramp rate 10°C/min

GC final temperature 250°C

GC final temperature hold time 1 min

Mass Spectrometer detectors Quadrupole-MS (Agilent)

Filament Voltage 1191V

Scan mass range 40-250

Data rate 50Hz

Ionisation -70eV

Grapes - Muscat

doi:10.17617/3.XTCCLC

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Elena Levin

Volcani Institute, Agricultural Research Center

Dr. Itay Maoz group; Postharvest science department

Sample in glass vial

20ml

Solid-Phase Microextraction (SPME)

Sample details

Title Grapes - Muscat

Date of collection 2015-09-04

Collection method Sample in glass vial

Collection volume (of the vial) 20ml

Did not weight No

Mass of object sample 2g

Sample storage before sampling? No

Material state (old) Crushed

Salts Sodium chloride

Incubation duration 1sec

Incubation temperature 25°C

Sampling method

Sampling method Solid-Phase Microextraction (SPME)

Robotic automation Yes

What platform? Centri PAL3

Sorbent type DVB/Carbon-WR/PDMS

Sorbent phase thickness 80um

Headspace equilibrium temperature 40°C

Headspace equilibrium time 30min

Extraction mode Yes

Extraction time 30min

Extraction temperature 40°C

Desorption time 5min

Desorption temperature 250°C

Vortex No

GC-MS

Column type HP-5ms

Column flow 23.823ml/min

Pressure 5.3171psi

Length 30m

Inner diameter 250mm

Film thickness 0.25μm

Carrier gas He

Temperature ramps

Number of ramps 2

GC initial temperature 40°C

GC initial temperature hold time 1min

GC first temperature ramp rate 5°C/min

GC second temperature 160°C

GC second temperature hold time 2min

GC second temperature ramp rate 10°C/min

GC final temperature 250°C

GC final temperature hold time 1 min

Mass Spectrometer detectors Quadrupole-MS (Agilent)

Filament Voltage 1191V

Scan mass range 40-250

Data rate 50Hz

Ionisation -70eV

Grapes - Crimson

doi:10.17617/3.R7J4BT

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Elena Levin

Volcani Institute, Agricultural Research Center

Dr. Itay Maoz group; Postharvest science department

Sample in glass vial

20ml

Solid-Phase Microextraction (SPME)

Sample details

Title Grapes - Crimson

Date of collection 2016-01-13

Collection method Sample in glass vial

Collection volume (of the vial) 20ml

Did not weight No

Mass of object sample 2g

Sample storage before sampling? No

Material state (old) Crushed

Salts Sodium chloride

Incubation duration 1sec

Incubation temperature 25°C

Sampling method

Sampling method Solid-Phase Microextraction (SPME)

Robotic automation Yes

What platform? Centri PAL3

Sorbent type DVB/Carbon-WR/PDMS

Sorbent phase thickness 80um

Headspace equilibrium temperature 40°C

Headspace equilibrium time 30min

Extraction mode Yes

Extraction time 30min

Extraction temperature 40°C

Desorption time 5min

Desorption temperature 250°C

Vortex No

GC-MS

Column type HP-5ms

Column flow 23.823ml/min

Pressure 5.3171psi

Length 30m

Inner diameter 250mm

Film thickness 0.25μm

Carrier gas He

Temperature ramps

Number of ramps 2

GC initial temperature 40°C

GC initial temperature hold time 1min

GC first temperature ramp rate 5°C/min

GC second temperature 160°C

GC second temperature hold time 2min

GC second temperature ramp rate 10°C/min

GC final temperature 250°C

GC final temperature hold time 1 min

Mass Spectrometer detectors Quadrupole-MS (Agilent)

Filament Voltage 1191V

Scan mass range 40-250

Data rate 50Hz

Ionisation -70eV

Grapes - Adominik

doi:10.17617/3.D4LFJS

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Elena Levin

Volcani Institute, Agricultural Research Center

Dr. Itay Maoz group; Postharvest science department

Sample in glass vial

20ml

Solid-Phase Microextraction (SPME)

Sample details

Title Grapes - Adominik

Date of collection 2015-08-26

Collection method Sample in glass vial

Collection volume (of the vial) 20ml

Did not weight No

Mass of object sample 2g

Sample storage before sampling? No

Material state (old) Crushed

Material state Fresh

Salts Sodium chloride

Incubation duration 1sec

Incubation temperature 25°C

Sampling method

Sampling method Solid-Phase Microextraction (SPME)

Robotic automation Yes

What platform? Centri PAL3

Sorbent type DVB/Carbon-WR/PDMS

Sorbent phase thickness 80um

Headspace equilibrium temperature 40°C

Headspace equilibrium time 30min

Extraction mode Yes

Extraction time 30min

Extraction temperature 40°C

Desorption time 5min

Desorption temperature 250°C

Vortex No

GC-MS

Column type HP-5ms

Column flow 23.823ml/min

Pressure 5.3171psi

Length 30m

Inner diameter 250mm

Film thickness 0.25μm

Carrier gas He

Temperature ramps

Number of ramps 2

GC initial temperature 40°C

GC initial temperature hold time 1min

GC first temperature ramp rate 5°C/min

GC second temperature 160°C

GC second temperature hold time 2min

GC second temperature ramp rate 10°C/min

GC final temperature 250°C

GC final temperature hold time 1 min

Mass Spectrometer detectors Quadrupole-MS (Agilent)

Filament Voltage 1191V

Scan mass range 40-250

Data rate 50Hz

Ionisation -70eV

Raspeberries

doi:10.17617/3.TKZIAD

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Elena Levin

Volcani Institute, Agricultural Research Center

Dr. Itay Maoz group; Postharvest science department

Sample in glass vial

20ml

Solid-Phase Microextraction (SPME)

Sample details

Title Raspeberries

Date of collection 2025-06-06

Collection method Sample in glass vial

Collection volume (of the vial) 20ml

Did not weight No

Mass of object sample 2g

Sample storage before sampling? No

Material state (old) Crushed

Salts Sodium chloride

Incubation duration 1sec

Incubation temperature 25°C

Sampling method

Sampling method Solid-Phase Microextraction (SPME)

Robotic automation Yes

What platform? Centri PAL3

Sorbent type DVB/Carbon-WR/PDMS

Sorbent phase thickness 80um

Headspace equilibrium temperature 40°C

Headspace equilibrium time 30min

Extraction mode Yes

Extraction time 30min

Extraction temperature 40°C

Desorption time 5min

Desorption temperature 250°C

Vortex No

GC-MS

Column type HP-5ms

Column flow 23.823ml/min

Pressure 5.3171psi

Length 30m

Inner diameter 250mm

Film thickness 0.25μm

Carrier gas He

Temperature ramps

Number of ramps 2

GC initial temperature 40°C

GC initial temperature hold time 1min

GC first temperature ramp rate 5°C/min

GC second temperature 160°C

GC second temperature hold time 2min

GC second temperature ramp rate 10°C/min

GC final temperature 250°C

GC final temperature hold time 5 min

Mass Spectrometer detectors Quadrupole-MS (Agilent)

Filament Voltage 1191V

Scan mass range 40-250

Data rate 50Hz

Ionisation -70eV

Yellow plums

doi:10.17617/3.DNCCMB

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Elena Levin

Volcani Institute, Agricultural Research Center

Dr. Itay Maoz group; Postharvest science department

Sample in glass vial

20ml

Solid-Phase Microextraction (SPME)

Sample details

Title Yellow plums

Date of collection 2024-11-13

Collection method Sample in glass vial

Collection volume (of the vial) 20ml

Did not weight No

Mass of object sample 2g

Sample storage before sampling? No

Material state (old) Crushed

Salts Sodium chloride

Incubation duration 1sec

Incubation temperature 25°C

Sampling method

Sampling method Solid-Phase Microextraction (SPME)

Robotic automation Yes

What platform? Centri PAL3

Sorbent type DVB/Carbon-WR/PDMS

Sorbent phase thickness 80um

Headspace equilibrium temperature 40°C

Headspace equilibrium time 30min

Extraction mode Yes

Extraction time 30min

Extraction temperature 40°C

Desorption time 5min

Desorption temperature 250°C

Vortex No

GC-MS

Column type HP-5ms

Column flow 23.823ml/min

Pressure 5.3171psi

Length 30m

Inner diameter 250mm

Film thickness 0.25μm

Carrier gas He

Temperature ramps

Number of ramps 2

GC initial temperature 40°C

GC initial temperature hold time 1min

GC first temperature ramp rate 5°C/min

GC second temperature 160°C

GC second temperature hold time 2min

GC second temperature ramp rate 10°C/min

GC final temperature 250°C

GC final temperature hold time 1 min

Mass Spectrometer detectors Quadrupole-MS (Agilent)

Filament Voltage 1191V

Scan mass range 40-250

Data rate 50Hz

Ionisation -70eV

Red Plums

doi:10.17617/3.5XMSHL

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Elena Levin

Volcani Institute, Agricultural Research Center

Dr. Itay Maoz group; Postharvest science department

Sample in glass vial

20ml

Solid-Phase Microextraction (SPME)

Sample details

Title Red Plums

Date of collection 2024-11-13

Collection method Sample in glass vial

Collection volume (of the vial) 20ml

Did not weight No

Mass of object sample 2g

Sample storage before sampling? No

Material state (old) Crushed

Salts Sodium chloride

Incubation duration 1sec

Incubation temperature 25°C

Sampling method

Sampling method Solid-Phase Microextraction (SPME)

Robotic automation No

Sorbent type DVB/Carbon-WR/PDMS

Sorbent phase thickness 80um

Headspace equilibrium temperature 40°C

Headspace equilibrium time 30min

Extraction mode Yes

Extraction time 30min

Extraction temperature 40°C

Desorption time 5min

Desorption temperature 250°C

Vortex No

GC-MS

Column type HP-5ms

Column flow 23.823ml/min

Pressure 5.3171psi

Length 30m

Inner diameter 250mm

Film thickness 0.25μm

Carrier gas He

Temperature ramps

Number of ramps 2

GC initial temperature 40°C

GC initial temperature hold time 1min

GC first temperature ramp rate 5°C/min

GC second temperature 160°C

GC second temperature hold time 2min

GC second temperature ramp rate 10°C/min

GC final temperature 250°C

GC final temperature hold time 1 min

Mass Spectrometer detectors Quadrupole-MS (Agilent)

Filament Voltage 1191V

Scan mass range 40-250

Data rate 50Hz

Ionisation -70eV

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