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Alfalfa Blossoms Honey Bottle 1

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Faith Zillinger

Michigan State University

Department of Food Science and Human Nutrition

Sample in glass vial

40ml

Solid-Phase Microextraction (SPME)

Sample details

Title Alfalfa Blossoms Honey Bottle 1

Project Floral Honey

Date of collection 2024-02-18

Citation https://doi.org/10.1111/1750-3841.17461

Collection method Sample in glass vial

Collection volume (of the vial) 40ml

Did not weight No

Mass of object sample 8g

Sample storage before sampling? No

Material state Fresh

Increase headspace sensitivity (“salting out”) {Empty}

Sampling method

Sampling method Solid-Phase Microextraction (SPME)

Robotic automation No

Sorbent type DVB/PDMS

Sorbent phase thickness 65um

Headspace equilibrium temperature 40°C

Headspace equilibrium time 10min

Extraction mode Yes

Extraction time 10min

Extraction temperature 35°C

Desorption time .5min

Desorption temperature 200°C

Vortex Yes

Vortex speed 1000rpm

GC-MS

Focusing trap Cooled Injection System

CIS low temperature -196°C

Trap split {Empty}

Column type HP-5

Column constant flow 1.5ml/min

Length 60m

Inner diameter .25mm

Film thickness .25μm

Carrier gas He

Temperature ramps

Number of ramps 1

GC initial temperature 40°C

GC initial temperature hold time .5min

GC first temperature ramp rate 43°C/min

GC final temperature 280°C

Mass Spectrometer detectors TOF (Leco)

Scan mass range 29-400

Data rate 20Hz

Ionisation -70eV

Orange Blossoms Honey Bottle 2

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Faith Zillinger

Michigan State University

Department of Food Science and Human Nutrition

Sample in glass vial

40ml

Solid-Phase Microextraction (SPME)

Sample details

Title Orange Blossoms Honey Bottle 2

Project Floral Honey

Date of collection 2024-02-18

Citation https://doi.org/10.1111/1750-3841.17461

Collection method Sample in glass vial

Collection volume (of the vial) 40ml

Did not weight No

Mass of object sample 8g

Sample storage before sampling? No

Material state Fresh

Increase headspace sensitivity (“salting out”) {Empty}

Sampling method

Sampling method Solid-Phase Microextraction (SPME)

Robotic automation No

Sorbent type DVB/PDMS

Sorbent phase thickness 65um

Headspace equilibrium temperature 40°C

Headspace equilibrium time 10min

Extraction mode Yes

Extraction time 10min

Extraction temperature 35°C

Desorption time .5min

Desorption temperature 200°C

Vortex Yes

Vortex speed 1000rpm

GC-MS

Focusing trap Cooled Injection System

CIS low temperature -196°C

Trap split {Empty}

Column type HP-5

Column constant flow 1.5ml/min

Length 60m

Inner diameter .25mm

Film thickness .25μm

Carrier gas He

Temperature ramps

Number of ramps 1

GC initial temperature 40°C

GC initial temperature hold time .5min

GC first temperature ramp rate 43°C/min

GC final temperature 280°C

Mass Spectrometer detectors TOF (Leco)

Scan mass range 29-400

Data rate 20Hz

Ionisation -70eV

Orange Blossoms Honey Bottle 1

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Faith Zillinger

Michigan State University

Department of Food Science and Human Nutrition

Sample in glass vial

40ml

Solid-Phase Microextraction (SPME)

Sample details

Title Orange Blossoms Honey Bottle 1

Project Floral Honey

Date of collection 2024-02-18

Citation https://doi.org/10.1111/1750-3841.17461

Collection method Sample in glass vial

Collection volume (of the vial) 40ml

Did not weight No

Mass of object sample 8g

Sample storage before sampling? No

Material state Fresh

Increase headspace sensitivity (“salting out”) {Empty}

Sampling method

Sampling method Solid-Phase Microextraction (SPME)

Robotic automation No

Sorbent type DVB/PDMS

Sorbent phase thickness 65um

Headspace equilibrium temperature 40°C

Headspace equilibrium time 10min

Extraction mode Yes

Extraction time 10min

Extraction temperature 35°C

Desorption time .5min

Desorption temperature 200°C

Vortex Yes

Vortex speed 1000rpm

GC-MS

Focusing trap Cooled Injection System

CIS low temperature -196°C

Trap split {Empty}

Column type HP-5

Column constant flow 1.5ml/min

Length 60m

Inner diameter .25mm

Film thickness .25μm

Carrier gas He

Temperature ramps

Number of ramps 1

GC initial temperature 40°C

GC initial temperature hold time .5min

GC first temperature ramp rate 43°C/min

GC final temperature 280°C

Mass Spectrometer detectors TOF (Leco)

Scan mass range 29-400

Data rate 20Hz

Ionisation -70eV

Clover Honey Bottle 2

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Faith Zillinger

Michigan State University

Department of Food Science and Human Nutrition

Sample in glass vial

40ml

Solid-Phase Microextraction (SPME)

Sample details

Title Clover Honey Bottle 2

Project Floral Honey

Date of collection 2024-02-18

Citation https://doi.org/10.1111/1750-3841.17461

Collection method Sample in glass vial

Collection volume (of the vial) 40ml

Did not weight No

Mass of object sample 8g

Sample storage before sampling? No

Material state Fresh

Increase headspace sensitivity (“salting out”) {Empty}

Sampling method

Sampling method Solid-Phase Microextraction (SPME)

Robotic automation No

Sorbent type DVB/PDMS

Sorbent phase thickness 65um

Headspace equilibrium temperature 40°C

Headspace equilibrium time 10min

Extraction mode Yes

Extraction time 10min

Extraction temperature 35°C

Desorption time .5min

Desorption temperature 200°C

Vortex Yes

Vortex speed 1000rpm

GC-MS

Focusing trap Cooled Injection System

CIS low temperature -196°C

Trap split {Empty}

Column type HP-5

Column constant flow 1.5ml/min

Length 60m

Inner diameter .25mm

Film thickness .25μm

Carrier gas He

Temperature ramps

Number of ramps 1

GC initial temperature 40°C

GC initial temperature hold time .5min

GC first temperature ramp rate 43°C/min

GC final temperature 280°C

Mass Spectrometer detectors TOF (Leco)

Scan mass range 29-400

Data rate 20Hz

Ionisation -70eV

Clover Honey Bottle 1

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Faith Zillinger

Michigan State University

Department of Food Science and Human Nutrition

Sample in glass vial

40ml

Solid-Phase Microextraction (SPME)

Sample details

Title Clover Honey Bottle 1

Project Floral Honey

Date of collection 2024-02-18

Citation https://doi.org/10.1111/1750-3841.17461

Collection method Sample in glass vial

Collection volume (of the vial) 40ml

Did not weight No

Mass of object sample 8g

Sample storage before sampling? No

Material state Fresh

Increase headspace sensitivity (“salting out”) {Empty}

Sampling method

Sampling method Solid-Phase Microextraction (SPME)

Robotic automation No

Sorbent type DVB/PDMS

Sorbent phase thickness 65um

Headspace equilibrium temperature 40°C

Headspace equilibrium time 10min

Extraction mode Yes

Extraction time 10min

Extraction temperature 35°C

Desorption time .5min

Desorption temperature 200°C

Vortex Yes

Vortex speed 1000rpm

GC-MS

Focusing trap Cooled Injection System

CIS low temperature -196°C

Trap split {Empty}

Column type HP-5

Column constant flow 1.5ml/min

Length 60m

Inner diameter .25mm

Film thickness .25μm

Carrier gas He

Temperature ramps

Number of ramps 1

GC initial temperature 40°C

GC initial temperature hold time .5min

GC first temperature ramp rate 43°C/min

GC final temperature 280°C

Mass Spectrometer detectors TOF (Leco)

Scan mass range 29-400

Data rate 20Hz

Ionisation -70eV

Wildflower Blossoms Honey Bottle 2

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Faith Zillinger

Michigan State University

Department of Food Science and Human Nutrition

Sample in glass vial

40ml

Solid-Phase Microextraction (SPME)

Sample details

Title Wildflower Blossoms Honey Bottle 2

Project Floral Honey

Date of collection 2024-02-18

Citation https://doi.org/10.1111/1750-3841.17461

Collection method Sample in glass vial

Collection volume (of the vial) 40ml

Did not weight No

Mass of object sample 8g

Sample storage before sampling? No

Material state Fresh

Increase headspace sensitivity (“salting out”) {Empty}

Sampling method

Sampling method Solid-Phase Microextraction (SPME)

Robotic automation No

Sorbent type DVB/PDMS

Sorbent phase thickness 65um

Headspace equilibrium temperature 40°C

Headspace equilibrium time 10min

Extraction mode Yes

Extraction time 10min

Extraction temperature 35°C

Desorption time .5min

Desorption temperature 200°C

Vortex Yes

Vortex speed 1000rpm

GC-MS

Focusing trap Cooled Injection System

CIS low temperature -196°C

Trap split {Empty}

Column type HP-5

Column constant flow 1.5ml/min

Length 60m

Inner diameter .25mm

Film thickness .25μm

Carrier gas He

Temperature ramps

Number of ramps 1

GC initial temperature 40°C

GC initial temperature hold time .5min

GC first temperature ramp rate 43°C/min

GC final temperature 280°C

Mass Spectrometer detectors TOF (Leco)

Scan mass range 29-400

Data rate 20Hz

Ionisation -70eV

Wildflower Blossoms Honey Bottle 1

Download

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Faith Zillinger

Michigan State University

Department of Food Science and Human Nutrition

Sample in glass vial

40ml

Solid-Phase Microextraction (SPME)

Sample details

Title Wildflower Blossoms Honey Bottle 1

Project Floral Honey

Date of collection 2024-02-18

Citation https://doi.org/10.1111/1750-3841.17461

Collection method Sample in glass vial

Collection volume (of the vial) 40ml

Did not weight No

Mass of object sample 8g

Sample storage before sampling? No

Material state Fresh

Increase headspace sensitivity (“salting out”) Yes

Salts Sodium chloride

Incubation duration 10sec

Incubation temperature 40°C

Sampling method

Sampling method Solid-Phase Microextraction (SPME)

Robotic automation No

Sorbent type DVB/PDMS

Sorbent phase thickness 65um

Headspace equilibrium temperature 40°C

Headspace equilibrium time 10min

Extraction mode Yes

Extraction time 10min

Extraction temperature 35°C

Desorption time .5min

Desorption temperature 200°C

Vortex Yes

Vortex speed 1000rpm

GC-MS

Focusing trap Cooled Injection System

CIS low temperature -196°C

Trap split No

Column type HP-5

Column constant flow 1.5ml/min

Length 60m

Inner diameter .25mm

Film thickness .25μm

Carrier gas He

Temperature ramps

Number of ramps 1

GC initial temperature 40°C

GC initial temperature hold time .5min

GC first temperature ramp rate 43°C/min

GC final temperature 280°C

Mass Spectrometer detectors TOF (Leco)

Scan mass range 29-400

Data rate 20Hz

Ionisation -70eV

Bluecrop Blueberry MeJA 10dpa 10min run

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Faith Zillinger

Michigan State University

Department of Food Science and Human Nutrition

Sample in glass vial

40ml

4.25g

Solid-Phase Microextraction (SPME)

Sample details

Title Bluecrop Blueberry MeJA 10dpa 10min run

Project PGR Bluberries

Date of collection 2025-12-10

Collection method Sample in glass vial

Collection volume (of the vial) 40ml

Did not weight No

Mass of object sample 4.25g

Sample storage before sampling? Yes

Sample storage temperature before sampling -80°C

Sample storage time before sampling 3350Hours

Material state Fresh, Crushed

Suppressing enzyme-driven changes No

Increase headspace sensitivity (“salting out”) Yes

Salts Sodium chloride

Incubation duration 300sec

Incubation temperature 50°C

Sampling method

Sampling method Solid-Phase Microextraction (SPME)

Robotic automation No

Sorbent type DVB/CAR/PDMS

Sorbent phase thickness 30um

Headspace equilibrium temperature 50°C

Headspace equilibrium time 5min

Extraction mode Yes

Extraction time 10min

Extraction temperature 50°C

Desorption time .5min

Desorption temperature 200°C

Vortex Yes

Vortex speed 1000rpm

GC-MS

Focusing trap Cooled Injection System

CIS low temperature -196°C

Trap split No

Column type DB-5

Column constant flow 0.15ml/min

Length 30m

Inner diameter .25mm

Film thickness 1μm

Carrier gas He

Temperature ramps

Number of ramps 3

GC initial temperature 40°C

GC initial temperature hold time 0.00min

GC first temperature ramp rate 43°C/min

GC second temperature 110°C

GC second temperature hold time 0.00min

GC second temperature ramp rate 20°C/min

GC third temperature 130°C

GC third temperature hold time 0.00min

GC third temperature ramp rate 48°C/min

GC final temperature 250°C

GC final temperature hold time 0.00 min

Mass Spectrometer detectors TOF (Leco)

Scan mass range 29-400

Data rate 20Hz

Ionisation -70eV

Bluecrop Blueberry ACC 10dpa 10min run

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Faith Zillinger

Michigan State University

Department of Food Science and Human Nutrition

Sample in glass vial

40ml

4.25g

Solid-Phase Microextraction (SPME)

Sample details

Title Bluecrop Blueberry ACC 10dpa 10min run

Project PGR Bluberries

Date of collection 2025-12-10

Collection method Sample in glass vial

Collection volume (of the vial) 40ml

Did not weight No

Mass of object sample 4.25g

Sample storage before sampling? Yes

Sample storage temperature before sampling -80°C

Sample storage time before sampling 3350Hours

Material state Fresh, Crushed

Suppressing enzyme-driven changes No

Increase headspace sensitivity (“salting out”) Yes

Salts Sodium chloride

Incubation duration 300sec

Incubation temperature 50°C

Sampling method

Sampling method Solid-Phase Microextraction (SPME)

Robotic automation No

Sorbent type DVB/CAR/PDMS

Sorbent phase thickness 30um

Headspace equilibrium temperature 50°C

Headspace equilibrium time 5min

Extraction mode Yes

Extraction time 10min

Extraction temperature 50°C

Desorption time .5min

Desorption temperature 200°C

Vortex Yes

Vortex speed 1000rpm

GC-MS

Focusing trap Cooled Injection System

CIS low temperature -196°C

Trap split No

Column type DB-5

Column constant flow 0.15ml/min

Length 30m

Inner diameter .25mm

Film thickness 1μm

Carrier gas He

Temperature ramps

Number of ramps 3

GC initial temperature 40°C

GC initial temperature hold time 0.00min

GC first temperature ramp rate 43°C/min

GC second temperature 110°C

GC second temperature hold time 0.00min

GC second temperature ramp rate 20°C/min

GC third temperature 130°C

GC third temperature hold time 0.00min

GC third temperature ramp rate 48°C/min

GC final temperature 250°C

GC final temperature hold time 0.00 min

Mass Spectrometer detectors TOF (Leco)

Scan mass range 29-400

Data rate 20Hz

Ionisation -70eV

Bluecrop Blueberry Control 10dpa 10min run

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Faith Zillinger

Michigan State University

Department of Food Science and Human Nutrition

Sample in glass vial

40ml

4.25g

Solid-Phase Microextraction (SPME)

Sample details

Title Bluecrop Blueberry Control 10dpa 10min run

Project PGR Bluberries

Date of collection 2025-12-09

Collection method Sample in glass vial

Collection volume (of the vial) 40ml

Did not weight No

Mass of object sample 4.25g

Sample storage before sampling? Yes

Sample storage temperature before sampling -80°C

Sample storage time before sampling 3336Hours

Material state Fresh, Crushed

Suppressing enzyme-driven changes No

Increase headspace sensitivity (“salting out”) Yes

Salts Sodium chloride

Incubation duration 300sec

Incubation temperature 50°C

Sampling method

Sampling method Solid-Phase Microextraction (SPME)

Robotic automation No

Sorbent type DVB/CAR/PDMS

Sorbent phase thickness 30um

Headspace equilibrium temperature 50°C

Headspace equilibrium time 5min

Extraction mode Yes

Extraction time 10min

Extraction temperature 50°C

Desorption time .5min

Desorption temperature 200°C

Vortex Yes

Vortex speed 1000rpm

GC-MS

Focusing trap Cooled Injection System

CIS low temperature -196°C

Trap split No

Column type DB-5

Column constant flow 0.15ml/min

Length 30m

Inner diameter .25mm

Film thickness 1μm

Carrier gas He

Temperature ramps

Number of ramps 3

GC initial temperature 40°C

GC initial temperature hold time 0.00min

GC first temperature ramp rate 43°C/min

GC second temperature 110°C

GC second temperature hold time 0.00min

GC second temperature ramp rate 20°C/min

GC third temperature 130°C

GC third temperature hold time 0.00min

GC third temperature ramp rate 48°C/min

GC final temperature 250°C

GC final temperature hold time 0.00 min

Mass Spectrometer detectors TOF (Leco)

Scan mass range 29-400

Data rate 20Hz

Ionisation -70eV