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Bluecrop Blueberry MeJA Treatment 5dpa 10s run

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Faith Zillinger

Michigan State University

Department of Food Science and Human Nutrition

Sample in glass vial

40ml

4.25g

Solid-Phase Microextraction (SPME)

Sample details

Title Bluecrop Blueberry MeJA Treatment 5dpa 10s run

Project PGR Bluberries

Date of collection 2025-12-09

Collection method Sample in glass vial

Collection volume (of the vial) 40ml

Did not weight No

Mass of object sample 4.25g

Sample storage before sampling? Yes

Sample storage temperature before sampling -80°C

Sample storage time before sampling 3453Hours

Material state Fresh, Crushed

Suppressing enzyme-driven changes No

Increase headspace sensitivity (“salting out”) Yes

Salts Sodium chloride

Incubation duration 300sec

Incubation temperature 50°C

Sampling method

Sampling method Solid-Phase Microextraction (SPME)

Robotic automation No

Sorbent type DVB/CAR/PDMS

Sorbent phase thickness 30um

Headspace equilibrium temperature 50°C

Headspace equilibrium time 5min

Extraction mode Yes

Extraction time .1min

Extraction temperature 50°C

Desorption time .5min

Desorption temperature 200°C

Vortex Yes

Vortex speed 1000rpm

GC-MS

Focusing trap Cooled Injection System

CIS low temperature -196°C

Trap split No

Column type DB-5

Column constant flow 0.15ml/min

Length 30m

Inner diameter .25mm

Film thickness 1μm

Carrier gas He

Temperature ramps

Number of ramps 2

GC initial temperature 40°C

GC initial temperature hold time 0.00min

GC first temperature ramp rate 43°C/min

GC second temperature 110°C

GC second temperature hold time 0.00min

GC second temperature ramp rate 20°C/min

GC final temperature 130°C

GC final temperature hold time 0.00 min

Mass Spectrometer detectors TOF (Leco)

Scan mass range 29-400

Data rate 20Hz

Ionisation -70eV

Bluecrop Blueberry ABA Treatment 5dpa 10s run

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Faith Zillinger

Michigan State University

Department of Food Science and Human Nutrition

Sample in glass vial

40ml

4.25g

Solid-Phase Microextraction (SPME)

Sample details

Title Bluecrop Blueberry ABA Treatment 5dpa 10s run

Project PGR Bluberries

Date of collection 2025-12-11

Collection method Sample in glass vial

Collection volume (of the vial) 40ml

Did not weight No

Mass of object sample 4.25g

Sample storage before sampling? Yes

Sample storage temperature before sampling -80°C

Sample storage time before sampling 3503Hours

Material state Fresh, Crushed

Suppressing enzyme-driven changes No

Increase headspace sensitivity (“salting out”) Yes

Salts Sodium chloride

Incubation duration 300sec

Incubation temperature 50°C

Sampling method

Sampling method Solid-Phase Microextraction (SPME)

Robotic automation No

Sorbent type DVB/CAR/PDMS

Sorbent phase thickness 30um

Headspace equilibrium temperature 50°C

Headspace equilibrium time 5min

Extraction mode Yes

Extraction time .1min

Extraction temperature 50°C

Desorption time .5min

Desorption temperature 200°C

Vortex Yes

Vortex speed 1000rpm

GC-MS

Focusing trap Cooled Injection System

CIS low temperature -196°C

Trap split No

Column type DB-5

Column constant flow 0.15ml/min

Length 30m

Inner diameter .25mm

Film thickness 1μm

Carrier gas He

Temperature ramps

Number of ramps 2

GC initial temperature 40°C

GC initial temperature hold time 0.00min

GC first temperature ramp rate 43°C/min

GC second temperature 110°C

GC second temperature hold time 0.00min

GC second temperature ramp rate 20°C/min

GC final temperature 130°C

GC final temperature hold time 0.00 min

Mass Spectrometer detectors TOF (Leco)

Scan mass range 29-400

Data rate 20Hz

Ionisation -70eV

Bluecrop Blueberry ACC Treatment 5dpa 10s run

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Faith Zillinger

Michigan State University

Department of Food Science and Human Nutrition

Sample in glass vial

40ml

4.25g

Solid-Phase Microextraction (SPME)

Sample details

Title Bluecrop Blueberry ACC Treatment 5dpa 10s run

Project PGR Bluberries

Date of collection 2025-12-11

Collection method Sample in glass vial

Collection volume (of the vial) 40ml

Did not weight No

Mass of object sample 4.25g

Sample storage before sampling? Yes

Sample storage temperature before sampling -80°C

Sample storage time before sampling 3502Hours

Material state Fresh, Crushed

Suppressing enzyme-driven changes No

Increase headspace sensitivity (“salting out”) Yes

Salts Sodium chloride

Incubation duration 300sec

Incubation temperature 50°C

Sampling method

Sampling method Solid-Phase Microextraction (SPME)

Robotic automation No

Sorbent type DVB/CAR/PDMS

Sorbent phase thickness 30um

Headspace equilibrium temperature 50°C

Headspace equilibrium time 5min

Extraction mode Yes

Extraction time .1min

Extraction temperature 50°C

Desorption time .5min

Desorption temperature 200°C

Vortex Yes

Vortex speed 1000rpm

GC-MS

Focusing trap Cooled Injection System

CIS low temperature -196°C

Trap split No

Column type DB-5

Column constant flow 0.15ml/min

Length 30m

Inner diameter .25mm

Film thickness 1μm

Carrier gas He

Temperature ramps

Number of ramps 2

GC initial temperature 40°C

GC initial temperature hold time 0.00min

GC first temperature ramp rate 43°C/min

GC second temperature 110°C

GC second temperature hold time 0.00min

GC second temperature ramp rate 20°C/min

GC final temperature 130°C

GC final temperature hold time 0.00 min

Mass Spectrometer detectors TOF (Leco)

Scan mass range 29-400

Data rate 20Hz

Ionisation -70eV

Bluecrop Blueberry Control 5dpa 10s run

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Faith Zillinger

Michigan State University

Department of Food Science and Human Nutrition

Sample in glass vial

40ml

4.25g

Solid-Phase Microextraction (SPME)

Sample details

Title Bluecrop Blueberry Control 5dpa 10s run

Project PGR Bluberries

Date of collection 2025-12-09

Collection method Sample in glass vial

Collection volume (of the vial) 40ml

Did not weight No

Mass of object sample 4.25g

Sample storage before sampling? Yes

Sample storage temperature before sampling -80°C

Sample storage time before sampling 3456Hours

Material state Fresh, Crushed

Suppressing enzyme-driven changes No

Increase headspace sensitivity (“salting out”) Yes

Salts Sodium chloride

Incubation duration 300sec

Incubation temperature 50°C

Sampling method

Sampling method Solid-Phase Microextraction (SPME)

Robotic automation No

Sorbent type DVB/CAR/PDMS

Sorbent phase thickness 30um

Headspace equilibrium temperature 50°C

Headspace equilibrium time 5min

Extraction mode Yes

Extraction time .1min

Extraction temperature 50°C

Desorption time .5min

Desorption temperature 200°C

Vortex Yes

Vortex speed 1000rpm

GC-MS

Focusing trap Cooled Injection System

CIS low temperature -196°C

Trap split No

Column type DB-5

Column constant flow 0.15ml/min

Length 30m

Inner diameter .25mm

Film thickness 1μm

Carrier gas He

Temperature ramps

Number of ramps 2

GC initial temperature 40°C

GC initial temperature hold time 0.00min

GC first temperature ramp rate 43°C/min

GC second temperature 110°C

GC second temperature hold time 0.00min

GC second temperature ramp rate 20°C/min

GC final temperature 130°C

GC final temperature hold time 0.00 min

Mass Spectrometer detectors TOF (Leco)

Scan mass range 29-400

Data rate 20Hz

Ionisation -70eV

Grapes - Thompson

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Elena Levin

Volcani Institute, Agricultural Research Center

Dr. Itay Maoz group; Postharvest science department

Sample in glass vial

20ml

Solid-Phase Microextraction (SPME)

Sample details

Title Grapes - Thompson

Project Insights into the chemosensory basis of flavor in table grapes

Date of collection 2015-10-13

Citation https://doi.org/10.1002/jsfa.10102

Collection method Sample in glass vial

Collection volume (of the vial) 20ml

Did not weight No

Mass of object sample 2g

Sample storage before sampling? No

Material state Crushed

Suppressing enzyme-driven changes Yes

Solution NaCl

Incubation duration 1sec

Incubation temperature 25°C

Increase headspace sensitivity (“salting out”) Yes

Salts Sodium chloride

Incubation duration 1sec

Incubation temperature 25°C

Sampling method

Sampling method Solid-Phase Microextraction (SPME)

Robotic automation Yes

What platform? Centri PAL3

Sorbent type DVB/Carbon-WR/PDMS

Sorbent phase thickness 80um

Headspace equilibrium temperature 40°C

Headspace equilibrium time 30min

Extraction mode Yes

Extraction time 30min

Extraction temperature 40°C

Desorption time 5min

Desorption temperature 250°C

Vortex No

GC-MS

Column type HP-5ms

Column constant flow 23.823ml/min

Column constant pressure 5.3171psi

Length 30m

Inner diameter 250mm

Film thickness 0.25μm

Carrier gas He

Temperature ramps

Number of ramps 2

GC initial temperature 40°C

GC initial temperature hold time 1min

GC first temperature ramp rate 5°C/min

GC second temperature 160°C

GC second temperature hold time 2min

GC second temperature ramp rate 10°C/min

GC final temperature 250°C

GC final temperature hold time 1 min

Mass Spectrometer detectors Quadrupole-MS (Agilent)

Scan mass range 40-250

Data rate 50Hz

Ionisation -70eV

Grapes - Superior

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Elena Levin

Volcani Institute, Agricultural Research Center

Dr. Itay Maoz group; Postharvest science department

Sample in glass vial

20ml

Solid-Phase Microextraction (SPME)

Sample details

Title Grapes - Superior

Project Insights into the chemosensory basis of flavor in table grapes

Date of collection 2015-08-27

Citation https://doi.org/10.1002/jsfa.10102

Collection method Sample in glass vial

Collection volume (of the vial) 20ml

Did not weight No

Mass of object sample 2g

Sample storage before sampling? No

Material state Crushed

Suppressing enzyme-driven changes Yes

Solution NaCl

Incubation duration 1sec

Incubation temperature 25°C

Increase headspace sensitivity (“salting out”) Yes

Salts Sodium chloride

Incubation duration 1sec

Incubation temperature 25°C

Sampling method

Sampling method Solid-Phase Microextraction (SPME)

Robotic automation Yes

What platform? Centri PAL3

Sorbent type DVB/Carbon-WR/PDMS

Sorbent phase thickness 80um

Headspace equilibrium temperature 40°C

Headspace equilibrium time 30min

Extraction mode Yes

Extraction time 30min

Extraction temperature 40°C

Desorption time 5min

Desorption temperature 250°C

Vortex No

GC-MS

Column type HP-5ms

Column constant flow 23.823ml/min

Column constant pressure 5.3171psi

Length 30m

Inner diameter 250mm

Film thickness 0.25μm

Carrier gas He

Temperature ramps

Number of ramps 2

GC initial temperature 40°C

GC initial temperature hold time 1min

GC first temperature ramp rate 5°C/min

GC second temperature 160°C

GC second temperature hold time 2min

GC second temperature ramp rate 10°C/min

GC final temperature 250°C

GC final temperature hold time 1 min

Mass Spectrometer detectors Quadrupole-MS (Agilent)

Scan mass range 40-250

Data rate 50Hz

Ionisation -70eV

Grapes - Sable seedless

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Elena Levin

Volcani Institute, Agricultural Research Center

Dr. Itay Maoz group; Postharvest science department

Sample in glass vial

20ml

Solid-Phase Microextraction (SPME)

Sample details

Title Grapes - Sable seedless

Project Insights into the chemosensory basis of flavor in table grapes

Date of collection 2015-08-25

Citation https://doi.org/10.1002/jsfa.10102

Collection method Sample in glass vial

Collection volume (of the vial) 20ml

Did not weight No

Mass of object sample 2g

Sample storage before sampling? No

Material state Crushed

Suppressing enzyme-driven changes Yes

Solution NaCl

Incubation duration 1sec

Incubation temperature 25°C

Increase headspace sensitivity (“salting out”) Yes

Salts Sodium chloride

Incubation duration 1sec

Incubation temperature 25°C

Sampling method

Sampling method Solid-Phase Microextraction (SPME)

Robotic automation Yes

What platform? Centri PAL3

Sorbent type DVB/Carbon-WR/PDMS

Sorbent phase thickness 80um

Headspace equilibrium temperature 40°C

Headspace equilibrium time 30min

Extraction mode Yes

Extraction time 30min

Extraction temperature 40°C

Desorption time 5min

Desorption temperature 250°C

Vortex No

GC-MS

Column type HP-5ms

Column constant flow 23.823ml/min

Column constant pressure 5.3171psi

Length 30m

Inner diameter 250mm

Film thickness 0.25μm

Carrier gas He

Temperature ramps

Number of ramps 2

GC initial temperature 40°C

GC initial temperature hold time 1min

GC first temperature ramp rate 5°C/min

GC second temperature 160°C

GC second temperature hold time 2min

GC second temperature ramp rate 10°C/min

GC final temperature 250°C

GC final temperature hold time 1 min

Mass Spectrometer detectors Quadrupole-MS (Agilent)

Scan mass range 40-250

Data rate 50Hz

Ionisation -70eV

Grapes - Quinerra

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Elena Levin

Volcani Institute, Agricultural Research Center

Dr. Itay Maoz group; Postharvest science department

Sample in glass vial

20ml

Solid-Phase Microextraction (SPME)

Sample details

Title Grapes - Quinerra

Project Insights into the chemosensory basis of flavor in table grapes

Date of collection 2015-09-04

Citation https://doi.org/10.1002/jsfa.10102

Collection method Sample in glass vial

Collection volume (of the vial) 20ml

Did not weight No

Mass of object sample 2g

Sample storage before sampling? No

Material state Crushed

Suppressing enzyme-driven changes Yes

Solution NaCl

Incubation duration 1sec

Incubation temperature 25°C

Increase headspace sensitivity (“salting out”) Yes

Salts Sodium chloride

Incubation duration 1sec

Incubation temperature 25°C

Sampling method

Sampling method Solid-Phase Microextraction (SPME)

Robotic automation Yes

What platform? Centri PAL3

Sorbent type DVB/Carbon-WR/PDMS

Sorbent phase thickness 80um

Headspace equilibrium temperature 40°C

Headspace equilibrium time 30min

Extraction mode Yes

Extraction time 30min

Extraction temperature 40°C

Desorption time 5min

Desorption temperature 250°C

Vortex No

GC-MS

Column type HP-5ms

Column constant flow 23.823ml/min

Column constant pressure 5.3171psi

Length 30m

Inner diameter 250mm

Film thickness 0.25μm

Carrier gas He

Temperature ramps

Number of ramps 2

GC initial temperature 40°C

GC initial temperature hold time 1min

GC first temperature ramp rate 5°C/min

GC second temperature 160°C

GC second temperature hold time 2min

GC second temperature ramp rate 10°C/min

GC final temperature 250°C

GC final temperature hold time 1 min

Mass Spectrometer detectors Quadrupole-MS (Agilent)

Scan mass range 40-250

Data rate 50Hz

Ionisation -70eV

Grapes - Muscat

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Elena Levin

Volcani Institute, Agricultural Research Center

Dr. Itay Maoz group; Postharvest science department

Sample in glass vial

20ml

Solid-Phase Microextraction (SPME)

Sample details

Title Grapes - Muscat

Project Insights into the chemosensory basis of flavor in table grapes

Date of collection 2015-09-04

Citation https://doi.org/10.1002/jsfa.10102

Collection method Sample in glass vial

Collection volume (of the vial) 20ml

Did not weight No

Mass of object sample 2g

Sample storage before sampling? No

Material state Crushed

Suppressing enzyme-driven changes Yes

Solution NaCl

Incubation duration 1sec

Incubation temperature 25°C

Increase headspace sensitivity (“salting out”) Yes

Salts Sodium chloride

Incubation duration 1sec

Incubation temperature 25°C

Sampling method

Sampling method Solid-Phase Microextraction (SPME)

Robotic automation Yes

What platform? Centri PAL3

Sorbent type DVB/Carbon-WR/PDMS

Sorbent phase thickness 80um

Headspace equilibrium temperature 40°C

Headspace equilibrium time 30min

Extraction mode Yes

Extraction time 30min

Extraction temperature 40°C

Desorption time 5min

Desorption temperature 250°C

Vortex No

GC-MS

Column type HP-5ms

Column constant flow 23.823ml/min

Column constant pressure 5.3171psi

Length 30m

Inner diameter 250mm

Film thickness 0.25μm

Carrier gas He

Temperature ramps

Number of ramps 2

GC initial temperature 40°C

GC initial temperature hold time 1min

GC first temperature ramp rate 5°C/min

GC second temperature 160°C

GC second temperature hold time 2min

GC second temperature ramp rate 10°C/min

GC final temperature 250°C

GC final temperature hold time 1 min

Mass Spectrometer detectors Quadrupole-MS (Agilent)

Scan mass range 40-250

Data rate 50Hz

Ionisation -70eV

Grapes - Crimson

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Elena Levin

Volcani Institute, Agricultural Research Center

Dr. Itay Maoz group; Postharvest science department

Sample in glass vial

20ml

Solid-Phase Microextraction (SPME)

Sample details

Title Grapes - Crimson

Project Insights into the chemosensory basis of flavor in table grapes

Date of collection 2016-01-13

Citation https://doi.org/10.1002/jsfa.10102

Collection method Sample in glass vial

Collection volume (of the vial) 20ml

Did not weight No

Mass of object sample 2g

Sample storage before sampling? No

Material state Crushed

Suppressing enzyme-driven changes Yes

Solution NaCl

Incubation duration 1sec

Incubation temperature 25°C

Increase headspace sensitivity (“salting out”) Yes

Salts Sodium chloride

Incubation duration 1sec

Incubation temperature 25°C

Sampling method

Sampling method Solid-Phase Microextraction (SPME)

Robotic automation Yes

What platform? Centri PAL3

Sorbent type DVB/Carbon-WR/PDMS

Sorbent phase thickness 80um

Headspace equilibrium temperature 40°C

Headspace equilibrium time 30min

Extraction mode Yes

Extraction time 30min

Extraction temperature 40°C

Desorption time 5min

Desorption temperature 250°C

Vortex No

GC-MS

Column type HP-5ms

Column constant flow 23.823ml/min

Column constant pressure 5.3171psi

Length 30m

Inner diameter 250mm

Film thickness 0.25μm

Carrier gas He

Temperature ramps

Number of ramps 2

GC initial temperature 40°C

GC initial temperature hold time 1min

GC first temperature ramp rate 5°C/min

GC second temperature 160°C

GC second temperature hold time 2min

GC second temperature ramp rate 10°C/min

GC final temperature 250°C

GC final temperature hold time 1 min

Mass Spectrometer detectors Quadrupole-MS (Agilent)

Scan mass range 40-250

Data rate 50Hz

Ionisation -70eV