Home | D2SmellData

Toothpaste

Download

view

Heather Spooner

University of Reading, Reading, Berkshire, United Kingdom

Department of Food and Nutritional Sciences

Sample in glass vial

18ml

0.9g

Solid-Phase Microextraction (SPME)

Sample details

Title Toothpaste

Project Parosmia Project

Date of collection 2020-08-10

Collection method Sample in glass vial

Collection volume (of the vial) 18ml

Did not weight No

Mass of object sample 0.9g

Sample storage before sampling? Yes

Sample storage temperature before sampling 4°C

Material state Fresh

Sampling method

Sampling method Solid-Phase Microextraction (SPME)

Robotic automation No

Sorbent type triple phase DVB/Carboxen/PDMS 1 cm
DVB 50 um Carboxen 30 um PDMS 30 um

Sorbent phase thickness 30um

Headspace equilibrium temperature 40°C

Headspace equilibrium time 20min

Extraction mode Yes

Extraction time 20min

Extraction temperature 40°C

Desorption time 20min

Desorption temperature 250°C

Vortex Yes

Vortex speed 500rpm

GC-MS

Column type HP-5 5% Phenyl Methyl Siloxan

Column constant flow 0.9ml/min

Length 30m

Inner diameter 0.25mm

Film thickness 1μm

Carrier gas He

Temperature ramps

Number of ramps 1

GC initial temperature 40°C

GC initial temperature hold time 2min

GC first temperature ramp rate 4°C/min

GC final temperature 250°C

GC final temperature hold time 6 min

Mass Spectrometer detectors Quadrupole MS 5975C (Agilent)

Scan mass range 20-280

Data rate 0.69Hz

Ionisation -70eV

Lime peel

Download

view

Heather Spooner

University of Reading, Reading, Berkshire, United Kingdom

Department of Food and Nutritional Sciences

Sample in glass vial

18ml

Solid-Phase Microextraction (SPME)

Sample details

Title Lime peel

Project Parosmia Project

Date of collection 2020-08-04

Collection method Sample in glass vial

Collection volume (of the vial) 18ml

Did not weight No

Mass of object sample 1g

Sample storage before sampling? Yes

Sample storage temperature before sampling 4°C

Material state Fresh

Sampling method

Sampling method Solid-Phase Microextraction (SPME)

Robotic automation No

Sorbent type triple phase DVB/Carboxen/PDMS 1 cm
DVB 50 um Carboxen 30 um PDMS 30 um

Sorbent phase thickness 30um

Headspace equilibrium temperature 40°C

Headspace equilibrium time 20min

Extraction mode Yes

Extraction time 20min

Extraction temperature 40°C

Desorption time 20min

Desorption temperature 250°C

Vortex Yes

Vortex speed 500rpm

GC-MS

Column type HP-5 5% Phenyl Methyl Siloxan

Column constant flow 0.9ml/min

Length 30m

Inner diameter 0.25mm

Film thickness 1μm

Carrier gas He

Temperature ramps

Number of ramps 1

GC initial temperature 40°C

GC initial temperature hold time 2min

GC first temperature ramp rate 4°C/min

GC final temperature 250°C

GC final temperature hold time 6 min

Mass Spectrometer detectors Quadrupole MS 5975C (Agilent)

Scan mass range 20-280

Data rate 0.69Hz

Ionisation -70eV

Lime juice and peel

Download

view

Heather Spooner

University of Reading, Reading, Berkshire, United Kingdom

Department of Food and Nutritional Sciences

Sample in glass vial

18ml

Solid-Phase Microextraction (SPME)

Sample details

Title Lime juice and peel

Project Parosmia Project

Date of collection 2020-08-04

Collection method Sample in glass vial

Collection volume (of the vial) 18ml

Did not weight No

Mass of object sample 1g

Sample storage before sampling? Yes

Sample storage temperature before sampling 4°C

Material state Fresh

Sampling method

Sampling method Solid-Phase Microextraction (SPME)

Robotic automation No

Sorbent type triple phase DVB/Carboxen/PDMS 1 cm
DVB 50 um Carboxen 30 um PDMS 30 um

Sorbent phase thickness 30um

Headspace equilibrium temperature 40°C

Headspace equilibrium time 20min

Extraction mode Yes

Extraction time 20min

Extraction temperature 40°C

Desorption time 20min

Desorption temperature 250°C

Vortex Yes

Vortex speed 500rpm

GC-MS

Column type HP-5 5% Phenyl Methyl Siloxan

Column constant flow 0.9ml/min

Length 30m

Inner diameter 0.25mm

Film thickness 1μm

Carrier gas He

Temperature ramps

Number of ramps 1

GC initial temperature 40°C

GC initial temperature hold time 2min

GC first temperature ramp rate 4°C/min

GC final temperature 250°C

GC final temperature hold time 6 min

Mass Spectrometer detectors Quadrupole MS 5975C (Agilent)

Scan mass range 20-280

Data rate 0.69Hz

Ionisation -70eV

Lime juice

Download

view

Heather Spooner

University of Reading, Reading, Berkshire, United Kingdom

Department of Food and Nutritional Sciences

Sample in glass vial

18ml

Solid-Phase Microextraction (SPME)

Sample details

Title Lime juice

Project Parosmia Project

Date of collection 2020-08-04

Collection method Sample in glass vial

Collection volume (of the vial) 18ml

Did not weight No

Mass of object sample 1g

Sample storage before sampling? Yes

Sample storage temperature before sampling 4°C

Material state Fresh

Sampling method

Sampling method Solid-Phase Microextraction (SPME)

Robotic automation No

Sorbent type triple phase DVB/Carboxen/PDMS 1 cm
DVB 50 um Carboxen 30 um PDMS 30 um

Sorbent phase thickness 30um

Headspace equilibrium temperature 40°C

Headspace equilibrium time 20min

Extraction mode Yes

Extraction time 20min

Extraction temperature 40°C

Desorption time 20min

Desorption temperature 250°C

Vortex Yes

Vortex speed 500rpm

GC-MS

Column type HP-5 5% Phenyl Methyl Siloxan

Column constant flow 0.9ml/min

Length 30m

Inner diameter 0.25mm

Film thickness 1μm

Carrier gas He

Temperature ramps

Number of ramps 1

GC initial temperature 40°C

GC initial temperature hold time 2min

GC first temperature ramp rate 4°C/min

GC final temperature 250°C

GC final temperature hold time 6 min

Mass Spectrometer detectors Quadrupole MS 5975C (Agilent)

Scan mass range 20-280

Data rate 0.69Hz

Ionisation -70eV

Cocoa drink

Download

view

Heather Spooner

University of Reading, Reading, Berkshire, United Kingdom

Department of Food and Nutritional Sciences

Sample in glass vial

18ml

Solid-Phase Microextraction (SPME)

Sample details

Title Cocoa drink

Project Parosmia Project

Date of collection 2020-08-04

Collection method Sample in glass vial

Collection volume (of the vial) 18ml

Did not weight No

Mass of object sample 4g

Sample storage before sampling? No

Material state In solution

Sampling method

Sampling method Solid-Phase Microextraction (SPME)

Robotic automation No

Sorbent type triple phase DVB/Carboxen/PDMS 1 cm
DVB 50 um Carboxen 30 um PDMS 30 um

Sorbent phase thickness 30um

Headspace equilibrium temperature 55°C

Headspace equilibrium time 20min

Extraction mode Yes

Extraction time 20min

Extraction temperature 55°C

Desorption time 20min

Desorption temperature 250°C

Vortex Yes

Vortex speed 500rpm

GC-MS

Column type HP-5 5% Phenyl Methyl Siloxan

Column constant flow 0.9ml/min

Length 30m

Inner diameter 0.25mm

Film thickness 1μm

Carrier gas He

Temperature ramps

Number of ramps 1

GC initial temperature 40°C

GC initial temperature hold time 2min

GC first temperature ramp rate 4°C/min

GC final temperature 250°C

GC final temperature hold time 6 min

Mass Spectrometer detectors Quadrupole MS 5975C (Agilent)

Scan mass range 20-280

Data rate 0.69Hz

Ionisation -70eV

Cocoa powder

Download

view

Heather Spooner

University of Reading, Reading, Berkshire, United Kingdom

Department of Food and Nutritional Sciences

Sample in glass vial

18ml

Solid-Phase Microextraction (SPME)

Sample details

Title Cocoa powder

Project Parosmia Project

Date of collection 2020-08-04

Collection method Sample in glass vial

Collection volume (of the vial) 18ml

Did not weight No

Mass of object sample 1g

Sample storage before sampling? Yes

Sample storage temperature before sampling 4°C

Material state Dried

Sampling method

Sampling method Solid-Phase Microextraction (SPME)

Robotic automation No

Sorbent type triple phase DVB/Carboxen/PDMS 1 cm
DVB 50 um Carboxen 30 um PDMS 30 um

Sorbent phase thickness 30um

Headspace equilibrium temperature 55°C

Headspace equilibrium time 20min

Extraction mode Yes

Extraction time 20min

Extraction temperature 55°C

Desorption time 20min

Desorption temperature 250°C

Vortex Yes

Vortex speed 500rpm

GC-MS

Column type HP-5 5% Phenyl Methyl Siloxan

Column constant flow 0.9ml/min

Length 30m

Inner diameter 0.25mm

Film thickness 1μm

Carrier gas He

Temperature ramps

Number of ramps 1

GC initial temperature 40°C

GC initial temperature hold time 2min

GC first temperature ramp rate 4°C/min

GC final temperature 250°C

GC final temperature hold time 6 min

Mass Spectrometer detectors Quadrupole MS 5975C (Agilent)

Scan mass range 20-280

Data rate 0.69Hz

Ionisation -70eV

Onion (raw frozen)

Download

view

Heather Spooner

University of Reading, Reading, Berkshire, United Kingdom

Department of Food and Nutritional Sciences

Sample in glass vial

18ml

0.3g

Solid-Phase Microextraction (SPME)

Sample details

Title Onion (raw frozen)

Project Parosmia Project

Date of collection 2020-07-22

Collection method Sample in glass vial

Collection volume (of the vial) 18ml

Did not weight No

Mass of object sample 0.3g

Sample storage before sampling? Yes

Sample storage temperature before sampling 4°C

Material state Chopped

Suppressing enzyme-driven changes No

Increase headspace sensitivity (“salting out”) No

Sampling method

Sampling method Solid-Phase Microextraction (SPME)

Robotic automation No

Sorbent type triple phase DVB/Carboxen/PDMS 1 cm
DVB 50 um Carboxen 30 um PDMS 30 um

Sorbent phase thickness 30um

Headspace equilibrium temperature 55°C

Headspace equilibrium time 0.167min

Extraction mode Yes

Extraction time 20min

Extraction temperature 55°C

Desorption time 20min

Desorption temperature 250°C

Vortex Yes

Vortex speed 500rpm

GC-MS

Column type HP-5 5% Phenyl Methyl Siloxan

Column constant flow 0.9ml/min

Length 30m

Inner diameter 0.25mm

Film thickness 1μm

Carrier gas He

Temperature ramps

Number of ramps 1

GC initial temperature 40°C

GC initial temperature hold time 2min

GC first temperature ramp rate 4°C/min

GC final temperature 250°C

GC final temperature hold time 6 min

Mass Spectrometer detectors Quadrupole MS 5975C (Agilent)

Scan mass range 20-280

Data rate 0.69Hz

Ionisation -70eV

Potato crisps

Download

view

Heather Spooner

University of Reading, Reading, Berkshire, United Kingdom

Department of Food and Nutritional Sciences

Sample in glass vial

18ml

1.5g

Solid-Phase Microextraction (SPME)

Sample details

Title Potato crisps

Project Parosmia Project

Date of collection 2020-07-14

Collection method Sample in glass vial

Collection volume (of the vial) 18ml

Did not weight No

Mass of object sample 1.5g

Sample storage before sampling? Yes

Sample storage temperature before sampling 4°C

Material state Crushed

Suppressing enzyme-driven changes No

Increase headspace sensitivity (“salting out”) Yes

Salts Sodium chloride

Sampling method

Sampling method Solid-Phase Microextraction (SPME)

Robotic automation No

Sorbent type triple phase DVB/Carboxen/PDMS 1 cm
DVB 50 um Carboxen 30 um PDMS 30 um

Sorbent phase thickness 30um

Headspace equilibrium temperature 55°C

Headspace equilibrium time 20min

Extraction mode Yes

Extraction time 20min

Extraction temperature 55°C

Desorption time 20min

Desorption temperature 250°C

Vortex Yes

Vortex speed 500rpm

GC-MS

Column type HP-5 5% Phenyl Methyl Siloxan

Column constant flow 0.9ml/min

Length 30m

Inner diameter 0.25mm

Film thickness 1μm

Carrier gas He

Temperature ramps

Number of ramps 1

GC initial temperature 40°C

GC initial temperature hold time 2min

GC first temperature ramp rate 4°C/min

GC final temperature 250°C

GC final temperature hold time 6 min

Mass Spectrometer detectors Quadrupole MS 5975C (Agilent)

Scan mass range 20-280

Data rate 0.69Hz

Ionisation -70eV

Peanut butter

Download

view

Heather Spooner

University of Reading, Reading, Berkshire, United Kingdom

Department of Food and Nutritional Sciences

Sample in glass vial

18ml

1.5g

Solid-Phase Microextraction (SPME)

Sample details

Title Peanut butter

Project Parosmia Project

Date of collection 2020-07-14

Collection method Sample in glass vial

Collection volume (of the vial) 18ml

Did not weight No

Mass of object sample 1.5g

Sample storage before sampling? Yes

Sample storage temperature before sampling 4°C

Material state Crushed

Suppressing enzyme-driven changes No

Increase headspace sensitivity (“salting out”) Yes

Salts Sodium chloride

Sampling method

Sampling method Solid-Phase Microextraction (SPME)

Robotic automation No

Sorbent type triple phase DVB/Carboxen/PDMS 1 cm
DVB 50 um Carboxen 30 um PDMS 30 um

Sorbent phase thickness 30um

Headspace equilibrium temperature 55°C

Headspace equilibrium time 20min

Extraction mode Yes

Extraction time 20min

Extraction temperature 55°C

Desorption time 20min

Desorption temperature 250°C

Vortex Yes

Vortex speed 500rpm

GC-MS

Column type HP-5 5% Phenyl Methyl Siloxan

Column constant flow 0.9ml/min

Length 30m

Inner diameter 0.25mm

Film thickness 1μm

Carrier gas He

Temperature ramps

Number of ramps 1

GC initial temperature 40°C

GC initial temperature hold time 2min

GC first temperature ramp rate 4°C/min

GC final temperature 250°C

GC final temperature hold time 6 min

Mass Spectrometer detectors Quadrupole MS 5975C (Agilent)

Scan mass range 20-280

Data rate 0.69Hz

Ionisation -70eV

Lettuce

Download

view

Heather Spooner

University of Reading, Reading, Berkshire, United Kingdom

Department of Food and Nutritional Sciences

Sample in glass vial

18ml

Solid-Phase Microextraction (SPME)

Sample details

Title Lettuce

Project Parosmia Project

Date of collection 2020-07-14

Collection method Sample in glass vial

Collection volume (of the vial) 18ml

Did not weight No

Mass of object sample 3g

Sample storage before sampling? Yes

Sample storage temperature before sampling 4°C

Material state Chopped

Suppressing enzyme-driven changes No

Increase headspace sensitivity (“salting out”) No

Sampling method

Sampling method Solid-Phase Microextraction (SPME)

Robotic automation No

Sorbent type triple phase DVB/Carboxen/PDMS 1 cm
DVB 50 um Carboxen 30 um PDMS 30 um

Sorbent phase thickness 30um

Headspace equilibrium temperature 40°C

Headspace equilibrium time 20min

Extraction mode Yes

Extraction time 20min

Extraction temperature 40°C

Desorption time 20min

Desorption temperature 250°C

Vortex Yes

Vortex speed 500rpm

GC-MS

Column type HP-5 5% Phenyl Methyl Siloxan

Column constant flow 0.9ml/min

Length 30m

Inner diameter 0.25mm

Film thickness 1μm

Carrier gas He

Temperature ramps

Number of ramps 1

GC initial temperature 40°C

GC initial temperature hold time 2min

GC first temperature ramp rate 4°C/min

GC final temperature 250°C

GC final temperature hold time 6 min

Mass Spectrometer detectors Quadrupole MS 5975C (Agilent)

Scan mass range 20-280

Data rate 0.69Hz

Ionisation -70eV

First page
Previous page
…
7
8
9
10
11
12
13
14
15
…
Next page
Last page