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toothpaste

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Eunyeong

Max Planck Institute for Chemistry

Jonathan Williams Group / Atmospheric Chemistry

Sample in glass vial

1000ml

Pump - sorbent tubes

Sample details

Title toothpaste

Project Object_smell

Date of collection 2026-01-21

Collection method Sample in glass vial

Collection volume (of the vial) 1000ml

Did not weight Yes

Sample storage before sampling? No

Material state Fresh

Sampling method

Sampling method Pump - sorbent tubes

Number of sorbents 2

Sorbent type Tenax TA

Sorbent amount 150

Mesh size 35/60

Sorbent type Carbograph 5

Sorbent amount 150

Mesh size 40/60

Sorbent tubes length for TD 89mm

Sorbent tube sampling volume 1000ml

Sorbent tube sampling flow rate 200ml/min

Sorbent tubes storage after sampling No

Ozone scrubber No

TDU type Markes TD100-xr

Tube desorption stages 1

Desorb time 5min

Desorb temperature 250°C

Trap flow 50ml/min

Split on 50ml/min

GC-MS

Focusing trap Markes focusing trap

Focusing trap sorbent-packed materials emissions

Desorb trap purge time 1min

Trap purge flow 50ml/min

Trap low temperature -20°C

Trap heating rate 45°C/s

Trap high (desorb) temperature 260°C

Trap desorb time 5min

Trap split Yes

Split flow 49ml/min

Column type ZB-624plus

Column constant flow 1ml/min

Column constant pressure 7.5psi

Length 30m

Inner diameter 0.25mm

Film thickness 1.4μm

Carrier gas He

Temperature ramps

Number of ramps 2

GC initial temperature 50°C

GC initial temperature hold time 5min

GC first temperature ramp rate 5°C/min

GC second temperature 150°C

GC second temperature hold time 5min

GC second temperature ramp rate 10°C/min

GC final temperature 250°C

GC final temperature hold time 5 min

Mass Spectrometer detectors QTOF (Agilent)

Scan mass range 29-350

Data rate 5Hz

Ionisation 70eV

Chicken stock powder

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Eunyeong

Max Planck Institute for Chemistry

Jonathan Williams Group / Atmospheric Chemistry

Sample in glass vial

1000ml

Pump - sorbent tubes

Sample details

Title Chicken stock powder

Project Object_smell

Date of collection 2026-01-21

Collection method Sample in glass vial

Collection volume (of the vial) 1000ml

Did not weight Yes

Sample storage before sampling? No

Material state Fresh

Sampling method

Sampling method Pump - sorbent tubes

Number of sorbents 2

Sorbent type Tenax TA

Sorbent amount 150

Mesh size 35/60

Sorbent type Carbograph 5

Sorbent amount 150

Mesh size 40/60

Sorbent tubes length for TD 89mm

Sorbent tube sampling volume 1000ml

Sorbent tube sampling flow rate 200ml/min

Sorbent tubes storage after sampling No

Ozone scrubber No

TDU type Markes TD100-xr

Tube desorption stages 1

Desorb time 5min

Desorb temperature 250°C

Trap flow 50ml/min

Split on 50ml/min

GC-MS

Focusing trap Markes focusing trap

Focusing trap sorbent-packed materials emissions

Desorb trap purge time 1min

Trap purge flow 50ml/min

Trap low temperature -20°C

Trap heating rate 45°C/s

Trap high (desorb) temperature 260°C

Trap desorb time 5min

Trap split Yes

Split flow 49ml/min

Column type ZB-624plus

Column constant flow 1ml/min

Column constant pressure 7.5psi

Length 30m

Inner diameter 0.25mm

Film thickness 1.4μm

Carrier gas He

Temperature ramps

Number of ramps 2

GC initial temperature 50°C

GC initial temperature hold time 5min

GC first temperature ramp rate 5°C/min

GC second temperature 150°C

GC second temperature hold time 5min

GC second temperature ramp rate 10°C/min

GC final temperature 250°C

GC final temperature hold time 5 min

Mass Spectrometer detectors QTOF (Agilent)

Scan mass range 29-350

Data rate 5Hz

Ionisation 70eV

candle

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Eunyeong

Max Planck Institute for Chemistry

Jonathan Williams Group / Atmospheric Chemistry

Sample in glass vial

1000ml

Pump - sorbent tubes

Sample details

Title candle

Project Object_smell

Date of collection 2026-01-21

Collection method Sample in glass vial

Collection volume (of the vial) 1000ml

Did not weight Yes

Sample storage before sampling? No

Material state Chopped

Suppressing enzyme-driven changes No

Increase headspace sensitivity (“salting out”) No

Sampling method

Sampling method Pump - sorbent tubes

Number of sorbents 2

Sorbent type Tenax TA

Sorbent amount 150

Mesh size 35/60

Sorbent type Carbograph 5

Sorbent amount 150

Mesh size 40/60

Sorbent tubes length for TD 89mm

Sorbent tube sampling volume 1000ml

Sorbent tube sampling flow rate 200ml/min

Sorbent tubes storage after sampling No

Ozone scrubber No

TDU type Markes TD100-xr

Tube desorption stages 1

Desorb time 5min

Desorb temperature 250°C

Trap flow 50ml/min

Split on 50ml/min

GC-MS

Focusing trap Markes focusing trap

Focusing trap sorbent-packed materials emissions

Desorb trap purge time 1min

Trap purge flow 50ml/min

Trap low temperature -20°C

Trap heating rate 45°C/s

Trap high (desorb) temperature 260°C

Trap desorb time 5min

Trap split Yes

Split flow 49ml/min

Column type ZB-624plus

Column constant flow 1ml/min

Column constant pressure 7.5psi

Length 30m

Inner diameter 0.25mm

Film thickness 1.4μm

Carrier gas He

Temperature ramps

Number of ramps 2

GC initial temperature 50°C

GC initial temperature hold time 5min

GC first temperature ramp rate 5°C/min

GC second temperature 150°C

GC second temperature hold time 5min

GC second temperature ramp rate 10°C/min

GC final temperature 250°C

GC final temperature hold time 5 min

Mass Spectrometer detectors QTOF (Agilent)

Scan mass range 29-350

Data rate 5Hz

Ionisation 70eV

Tomato Harvest 2 4C storage Day 8

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Jane Parker

University of Reading, Reading, Berkshire, United Kingdom

Department of Food and Nutritional Sciences

Sample in glass vial

18ml

Solid-Phase Microextraction (SPME)

Sample details

Title Tomato Harvest 2 4C storage Day 8

Project Tomato Storage Harvest 2

Date of collection 2017-03-31

Citation MSc Thesis 2017 Artem Trufanov

Collection method Sample in glass vial

Collection volume (of the vial) 18ml

Did not weight No

Mass of object sample 5g

Sample storage before sampling? No

Material state Chopped

Suppressing enzyme-driven changes Yes

Solution The fruit were taken off the scale and blended for 30 s, stopped for 90 s (to allow some initial enzyme activity during this time). After blending part a saturated CaCl2 solution (80g CaCl2 / 100 g water) added to the homogenate enzymes; with proportion 1

Increase headspace sensitivity (“salting out”) No

Sampling method

Sampling method Solid-Phase Microextraction (SPME)

Robotic automation Yes

What platform? CombiPal

Sorbent type triple phase DVB/Carboxen/PDMS 1 cm
DVB 50 um Carboxen 30 um PDMS 30 um

Sorbent phase thickness 30um

Headspace equilibrium temperature 37°C

Headspace equilibrium time 10min

Extraction mode Yes

Extraction time 15min

Extraction temperature 37°C

Desorption time 10min

Desorption temperature 250°C

Vortex Yes

Vortex speed 500rpm

GC-MS

Column type Zebron DB5 MSi

Column constant flow 0.9ml/min

Length 30m

Inner diameter 0.25mm

Film thickness 1μm

Carrier gas He

Temperature ramps

Number of ramps 1

GC initial temperature 40°C

GC initial temperature hold time 5min

GC first temperature ramp rate 6°C/min

GC final temperature 260°C

GC final temperature hold time 0 min

Mass Spectrometer detectors Quadrupole MS 5975C (Agilent)

Scan mass range 20-280

Data rate 5.2Hz

Ionisation -70eV

Tomato Harvest 2 10C storage Day 8

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Jane Parker

University of Reading, Reading, Berkshire, United Kingdom

Department of Food and Nutritional Sciences

Sample in glass vial

18ml

Solid-Phase Microextraction (SPME)

Sample details

Title Tomato Harvest 2 10C storage Day 8

Project Tomato Storage Harvest 2

Date of collection 2017-03-31

Citation MSc Thesis 2017 Artem Trufanov

Collection method Sample in glass vial

Collection volume (of the vial) 18ml

Did not weight No

Mass of object sample 5g

Sample storage before sampling? No

Material state Chopped

Suppressing enzyme-driven changes Yes

Increase headspace sensitivity (“salting out”) No

Sampling method

Sampling method Solid-Phase Microextraction (SPME)

Robotic automation Yes

What platform? CombiPal

Sorbent type triple phase DVB/Carboxen/PDMS 1 cm
DVB 50 um Carboxen 30 um PDMS 30 um

Sorbent phase thickness 30um

Headspace equilibrium temperature 37°C

Headspace equilibrium time 10min

Extraction mode Yes

Extraction time 15min

Extraction temperature 37°C

Desorption time 10min

Desorption temperature 250°C

Vortex Yes

Vortex speed 500rpm

GC-MS

Column type Zebron DB5 MSi

Column constant flow 0.9ml/min

Length 30m

Inner diameter 0.25mm

Film thickness 1μm

Carrier gas He

Temperature ramps

Number of ramps 1

GC initial temperature 40°C

GC initial temperature hold time 5min

GC first temperature ramp rate 6°C/min

GC final temperature 260°C

GC final temperature hold time 0 min

Mass Spectrometer detectors Quadrupole MS 5975C (Agilent)

Scan mass range 20-280

Data rate 5.2Hz

Ionisation -70eV

Tomato Harvest 2 20C storage Day 8

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Jane Parker

University of Reading, Reading, Berkshire, United Kingdom

Department of Food and Nutritional Sciences

Sample in glass vial

18ml

Solid-Phase Microextraction (SPME)

Sample details

Title Tomato Harvest 2 20C storage Day 8

Project Tomato Storage Harvest 2

Date of collection 2017-03-31

Citation MSc Thesis 2017 Artem Trufanov

Collection method Sample in glass vial

Collection volume (of the vial) 18ml

Did not weight No

Mass of object sample 5g

Sample storage before sampling? No

Material state Chopped

Suppressing enzyme-driven changes Yes

Increase headspace sensitivity (“salting out”) No

Sampling method

Sampling method Solid-Phase Microextraction (SPME)

Robotic automation Yes

What platform? CombiPal

Sorbent type triple phase DVB/Carboxen/PDMS 1 cm
DVB 50 um Carboxen 30 um PDMS 30 um

Sorbent phase thickness 30um

Headspace equilibrium temperature 37°C

Headspace equilibrium time 10min

Extraction mode Yes

Extraction time 15min

Extraction temperature 37°C

Desorption time 10min

Desorption temperature 250°C

Vortex Yes

Vortex speed 500rpm

GC-MS

Column type Zebron DB5 MSi

Column constant flow 0.9ml/min

Length 30m

Inner diameter 0.25mm

Film thickness 1μm

Carrier gas He

Temperature ramps

Number of ramps 1

GC initial temperature 40°C

GC initial temperature hold time 5min

GC first temperature ramp rate 6°C/min

GC final temperature 260°C

GC final temperature hold time 0 min

Mass Spectrometer detectors Quadrupole MS 5975C (Agilent)

Scan mass range 20-280

Data rate 5.2Hz

Ionisation -70eV

Tomato Harvest 2 20C storage Day 4

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Jane Parker

University of Reading, Reading, Berkshire, United Kingdom

Department of Food and Nutritional Sciences

Sample in glass vial

18ml

Solid-Phase Microextraction (SPME)

Sample details

Title Tomato Harvest 2 20C storage Day 4

Project Tomato Storage Harvest 2

Date of collection 2017-03-31

Citation MSc Thesis 2017 Artem Trufanov

Collection method Sample in glass vial

Collection volume (of the vial) 18ml

Did not weight No

Mass of object sample 5g

Sample storage before sampling? No

Material state Chopped

Suppressing enzyme-driven changes Yes

Increase headspace sensitivity (“salting out”) No

Sampling method

Sampling method Solid-Phase Microextraction (SPME)

Robotic automation Yes

What platform? CombiPal

Sorbent type triple phase DVB/Carboxen/PDMS 1 cm
DVB 50 um Carboxen 30 um PDMS 30 um

Sorbent phase thickness 30um

Headspace equilibrium temperature 37°C

Headspace equilibrium time 10min

Extraction mode Yes

Extraction time 15min

Extraction temperature 37°C

Desorption time 10min

Desorption temperature 250°C

Vortex Yes

Vortex speed 500rpm

GC-MS

Column type Zebron DB5 MSi

Column constant flow 0.9ml/min

Length 30m

Inner diameter 0.25mm

Film thickness 1μm

Carrier gas He

Temperature ramps

Number of ramps 1

GC initial temperature 40°C

GC initial temperature hold time 5min

GC first temperature ramp rate 6°C/min

GC final temperature 260°C

GC final temperature hold time 0 min

Mass Spectrometer detectors Quadrupole MS 5975C (Agilent)

Scan mass range 20-280

Data rate 5.2Hz

Ionisation -70eV

Tomato Harvest 2 10C storage Day 4

Download

view

Jane Parker

University of Reading, Reading, Berkshire, United Kingdom

Department of Food and Nutritional Sciences

Sample in glass vial

18ml

Solid-Phase Microextraction (SPME)

Sample details

Title Tomato Harvest 2 10C storage Day 4

Project Tomato Storage Harvest 2

Date of collection 2017-03-31

Citation MSc Thesis 2017 Artem Trufanov

Collection method Sample in glass vial

Collection volume (of the vial) 18ml

Did not weight No

Mass of object sample 5g

Sample storage before sampling? No

Material state Chopped

Suppressing enzyme-driven changes Yes

Increase headspace sensitivity (“salting out”) No

Sampling method

Sampling method Solid-Phase Microextraction (SPME)

Robotic automation Yes

What platform? CombiPal

Sorbent type triple phase DVB/Carboxen/PDMS 1 cm
DVB 50 um Carboxen 30 um PDMS 30 um

Sorbent phase thickness 30um

Headspace equilibrium temperature 37°C

Headspace equilibrium time 10min

Extraction mode Yes

Extraction time 15min

Extraction temperature 37°C

Desorption time 10min

Desorption temperature 250°C

Vortex Yes

Vortex speed 500rpm

GC-MS

Column type Zebron DB5 MSi

Column constant flow 0.9ml/min

Length 30m

Inner diameter 0.25mm

Film thickness 1μm

Carrier gas He

Temperature ramps

Number of ramps 1

GC initial temperature 40°C

GC initial temperature hold time 5min

GC first temperature ramp rate 6°C/min

GC final temperature 260°C

GC final temperature hold time 0 min

Mass Spectrometer detectors Quadrupole MS 5975C (Agilent)

Scan mass range 20-280

Data rate 5.2Hz

Ionisation -70eV

Tomato Harvest 2 Day 0

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Jane Parker

University of Reading, Reading, Berkshire, United Kingdom

Department of Food and Nutritional Sciences

Sample in glass vial

18ml

Solid-Phase Microextraction (SPME)

Sample details

Title Tomato Harvest 2 Day 0

Project Tomato Storage Harvest 2

Date of collection 2017-03-28

Citation MSc Thesis 2017 Artem Trufanov

Collection method Sample in glass vial

Collection volume (of the vial) 18ml

Did not weight No

Mass of object sample 5g

Sample storage before sampling? No

Material state Chopped

Suppressing enzyme-driven changes Yes

Increase headspace sensitivity (“salting out”) No

Sampling method

Sampling method Solid-Phase Microextraction (SPME)

Robotic automation Yes

What platform? CombiPal

Sorbent type triple phase DVB/Carboxen/PDMS 1 cm
DVB 50 um Carboxen 30 um PDMS 30 um

Sorbent phase thickness 30um

Headspace equilibrium temperature 37°C

Headspace equilibrium time 10min

Extraction mode Yes

Extraction time 15min

Extraction temperature 37°C

Desorption time 10min

Desorption temperature 250°C

Vortex Yes

Vortex speed 500rpm

GC-MS

Column type Zebron DB5 MSi

Column constant flow 0.9ml/min

Length 30m

Inner diameter 0.25mm

Film thickness 1μm

Carrier gas He

Temperature ramps

Number of ramps 1

GC initial temperature 40°C

GC initial temperature hold time 5min

GC first temperature ramp rate 6°C/min

GC final temperature 260°C

GC final temperature hold time 0 min

Mass Spectrometer detectors Quadrupole MS 5975C (Agilent)

Scan mass range 20-280

Data rate 5.2Hz

Ionisation -70eV

Tomato Day 4 storage 20C

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Jane Parker

University of Reading, Reading, Berkshire, United Kingdom

Department of Food and Nutritional Sciences

Sample in glass vial

18ml

Solid-Phase Microextraction (SPME)

Sample details

Title Tomato Day 4 storage 20C

Project Tomato Storage

Date of collection 2017-03-20

Citation MSc Thesis 2017 Artem Trufanov

Collection method Sample in glass vial

Collection volume (of the vial) 18ml

Did not weight No

Mass of object sample 5g

Sample storage before sampling? No

Material state Chopped

Suppressing enzyme-driven changes Yes

Increase headspace sensitivity (“salting out”) No

Sampling method

Sampling method Solid-Phase Microextraction (SPME)

Robotic automation Yes

What platform? CombiPal

Sorbent type triple phase DVB/Carboxen/PDMS 1 cm
DVB 50 um Carboxen 30 um PDMS 30 um

Sorbent phase thickness 30um

Headspace equilibrium temperature 37°C

Headspace equilibrium time 10min

Extraction mode Yes

Extraction time 15min

Extraction temperature 37°C

Desorption time 10min

Desorption temperature 250°C

Vortex Yes

Vortex speed 500rpm

GC-MS

Column type Zebron DB5 MSi

Column constant flow 0.9ml/min

Length 30m

Inner diameter 0.25mm

Film thickness 1μm

Carrier gas He

Temperature ramps

Number of ramps 1

GC initial temperature 40°C

GC initial temperature hold time 5min

GC first temperature ramp rate 6°C/min

GC final temperature 260°C

GC final temperature hold time 0 min

Mass Spectrometer detectors Quadrupole MS 5975C (Agilent)

Scan mass range 20-280

Data rate 5.2Hz

Ionisation -70eV

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