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Ginger (Zingiber officinale)

doi:10.17617/3.VSHPYY

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Tali Weiss

Weizmann Institute of Science

The department of Brain Sciences

Sample in glass vial

2ml

Static headspace using syringe injection

Sample details

Title Ginger (Zingiber officinale)

Collection method Sample in glass vial

Collection volume 2ml

Did not weight Yes

Sample storage before sampling? Yes

Sample storage temperature before sampling 25°C

Sample storage time before sampling 0.1Hours

Sampling method

Sampling method Static headspace using syringe injection

Robotic automation Yes

What platform? Centri 360

Sampling make up gas N2

Syringe volume 5ml

Heat Syringe 50°C

Total sampling volume 15ml

Enrich sample on cold trap Yes

Total number of injections 3

Enrichment delay 1min

Incubation before sampling Yes

Incubation time 0.5min

Incubation temperature 45°C

Agitation during the incubation period Yes

Injector temperature 250°C

Injection Time 2min

Incubation during sampling No

GC-MS

Focusing trap Markes focusing trap

Focusing trap sorbent-packed UNITY-T12ME-2S Material emissions, C4 - C32

Desorb trap purge time 0.5min

Trap purge flow 40ml/min

Trap low temperature 10°C

Trap heating rate 100°C/s

Trap high (desorb) temperature 250°C

Trap desorb time 2min

Trap split Yes

Split flow 30ml/min

Column type DB-WAX-UI

Column flow 1.29ml/min

Pressure 14psi

Length 30m

Inner diameter 0.25mm

Film thickness 0.5μm

Carrier gas He

Temperature ramps

Number of ramps 1

GC initial temperature 35°C

GC initial temperature hold time 1min

GC first temperature ramp rate 10°C/min

GC final temperature 220°C

GC final temperature hold time 1 min

Mass Spectrometer detectors BenchTOF2 (SepSolve)

Filament Voltage 1.6V

Scan mass range 35-300

Data rate 8Hz

Ionisation -70eV

Marker

doi:10.17617/3.YLSPSS

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Eunyeong

Max Planck Institute for Chemistry

Jonathan Williams Group / Atmospheric Chemistry

capture a gas from the object

1000ml

Dynamic headspace

Sample details

Title Marker

Collection method capture a gas from the object

Collection volume 1000ml

Did not weight Yes

Sample storage before sampling? No

Sampling method

Sampling method Dynamic headspace

Robotic automation No

Sorbent tubes for TD 89mm

Mesh Sizes in Absorbent Tubes 40-60

Type and amount of sorbents in sorbent tube 150 mg carbograph 5 and 150 mg of Tenax TA

Sorbent tube sampling volume 1000ml

Sorbent tube sampling flow rate 200ml/min

Sorbent tubes storage after sampling No

Sampling make up gas Ambient air

Dry purge time 0min

Dry purge flow 0ml/min

TDU type Markes TD100-xr

Tube desorption stages 1

Desorb time 5min

Desorb temperature 250°C

Trap flow 50ml/min

Split on 50ml/min

GC-MS

Focusing trap Markes focusing trap

Focusing trap sorbent-packed materials emissions

Desorb trap purge time 1min

Trap purge flow 50ml/min

Trap low temperature -20°C

Trap heating rate 45°C/s

Trap high (desorb) temperature 260°C

Trap desorb time 5min

Trap split Yes

Split flow 49ml/min

Column type ZB-624plus

Column flow 1ml/min

Pressure 7.5psi

Length 30m

Inner diameter 0.25mm

Film thickness 1.4μm

Carrier gas He

Temperature ramps

Number of ramps 2

GC initial temperature 50°C

GC initial temperature hold time 5min

GC first temperature ramp rate 5°C/min

GC second temperature 150°C

GC second temperature hold time 5min

GC second temperature ramp rate 10°C/min

GC final temperature 250°C

GC final temperature hold time 5 min

Mass Spectrometer detectors QTOF (Agilent)

Scan mass range 29-350

Data rate 5Hz

Ionisation 70eV

Marker

doi:10.17617/3.IWILDO

Download

Eunyeong

Max Planck Institute for Chemistry

Jonathan Williams Group / Atmospheric Chemistry

capture a gas from the object

1000ml

Dynamic headspace

Sample details

Title Marker

Collection method capture a gas from the object

Collection volume 1000ml

Did not weight Yes

Sample storage before sampling? No

Sampling method

Sampling method Dynamic headspace

Robotic automation No

Sorbent tubes for TD 89mm

Mesh Sizes in Absorbent Tubes 40-60

Type and amount of sorbents in sorbent tube 150 mg carbograph 5 and 150 mg of Tenax TA

Sorbent tube sampling volume 1000ml

Sorbent tube sampling flow rate 200ml/min

Sorbent tubes storage after sampling No

Sampling make up gas Ambient air

Dry purge time 0min

Dry purge flow 0ml/min

TDU type Markes TD100-xr

Tube desorption stages 1

Desorb time 5min

Desorb temperature 250°C

Trap flow 50ml/min

Split on 50ml/min

GC-MS

Focusing trap Markes focusing trap

Focusing trap sorbent-packed materials emissions

Desorb trap purge time 1min

Trap purge flow 50ml/min

Trap low temperature -20°C

Trap heating rate 45°C/s

Trap high (desorb) temperature 260°C

Trap desorb time 5min

Trap split Yes

Split flow 49ml/min

Column type ZB-624plus

Column flow 1ml/min

Pressure 7.5psi

Length 30m

Inner diameter 0.25mm

Film thickness 1.4μm

Carrier gas He

Temperature ramps

Number of ramps 2

GC initial temperature 50°C

GC initial temperature hold time 5min

GC first temperature ramp rate 5°C/min

GC second temperature 150°C

GC second temperature hold time 5min

GC second temperature ramp rate 10°C/min

GC final temperature 250°C

GC final temperature hold time 5 min

Mass Spectrometer detectors QTOF (Agilent)

Scan mass range 29-350

Data rate 5Hz

Ionisation 70eV

Black Tea

doi:10.17617/3.XBJ4T7

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Tali Weiss

Weizmann Institute of Science

The department of Brain Sciences

Sample in glass vial

20ml

0.4g

Static headspace using syringe injection

Sample details

Title Black Tea

Collection method Sample in glass vial

Collection volume 20ml

Did not weight No

Mass of object sample 0.4g

Sample storage before sampling? Yes

Sample storage temperature before sampling 25°C

Sample storage time before sampling 0.1Hours

Sampling method

Sampling method Static headspace using syringe injection

Robotic automation Yes

What platform? Centri 360

Sampling make up gas N2

Syringe volume 5ml

Heat Syringe 55°C

Total sampling volume 30ml

Enrich sample on cold trap Yes

Total number of injections 6

Enrichment delay 1min

Incubation before sampling Yes

Incubation time 0.5min

Incubation temperature 50°C

Agitation during the incubation period Yes

Injector temperature 250°C

Injection Time 2min

Incubation during sampling No

GC-MS

Focusing trap Markes focusing trap

Focusing trap sorbent-packed UNITY-T12ME-2S Material emissions, C4 - C32

Desorb trap purge time 0.5min

Trap purge flow 40ml/min

Trap low temperature 10°C

Trap heating rate 100°C/s

Trap high (desorb) temperature 250°C

Trap desorb time 2min

Trap split Yes

Split flow 40ml/min

Column type DB-WAX-UI

Column flow 1.29ml/min

Pressure 14psi

Length 30m

Inner diameter 0.25mm

Film thickness 0.5μm

Carrier gas He

Temperature ramps

Number of ramps 1

GC initial temperature 35°C

GC initial temperature hold time 1min

GC first temperature ramp rate 10°C/min

GC final temperature 220°C

GC final temperature hold time 1 min

Mass Spectrometer detectors BenchTOF2 (SepSolve)

Filament Voltage 1.6V

Scan mass range 35-300

Data rate 8Hz

Ionisation -70eV

Rotten Banana

doi:10.17617/3.QT4BZC

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Tali Weiss

Weizmann Institute of Science

The department of Brain Sciences

Sample in glass vial

20ml

Static headspace using syringe injection

Sample details

Title Rotten Banana

Collection method Sample in glass vial

Collection volume 20ml

Did not weight Yes

Sample storage before sampling? Yes

Sample storage temperature before sampling 25°C

Sample storage time before sampling 168Hours

Sampling method

Sampling method Static headspace using syringe injection

Robotic automation Yes

What platform? Centri 360

Sampling make up gas N2

Syringe volume 5ml

Heat Syringe 45°C

Total sampling volume 3ml

Enrich sample on cold trap No

Incubation before sampling Yes

Incubation time 0.5min

Incubation temperature 40°C

Agitation during the incubation period No

Injector temperature 250°C

Injection Time 2min

Incubation during sampling No

GC-MS

Focusing trap Markes focusing trap

Focusing trap sorbent-packed UNITY-T12ME-2S Material emissions, C4 - C32

Desorb trap purge time 0.5min

Trap purge flow 40ml/min

Trap low temperature 10°C

Trap heating rate 100°C/s

Trap high (desorb) temperature 250°C

Trap desorb time 2min

Trap split Yes

Split flow 80ml/min

Column type DB-WAX-UI

Column flow 1.29ml/min

Pressure 14psi

Length 30m

Inner diameter 0.25mm

Film thickness 0.5μm

Carrier gas He

Temperature ramps

Number of ramps 1

GC initial temperature 35°C

GC initial temperature hold time 1min

GC first temperature ramp rate 10°C/min

GC final temperature 220°C

GC final temperature hold time 1 min

Mass Spectrometer detectors BenchTOF2 (SepSolve)

Filament Voltage 1.6V

Scan mass range 35-300

Data rate 8Hz

Ionisation -70eV

Dark Chocolate 90%

doi:10.17617/3.SA15EA

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Tali Weiss

Weizmann Institute of Science

The department of Brain Sciences

Sample in glass vial

20ml

Static headspace using syringe injection

Sample details

Title Dark Chocolate 90%

Collection method Sample in glass vial

Collection volume 20ml

Did not weight No

Mass of object sample 3g

Sample storage before sampling? No

Sampling method

Sampling method Static headspace using syringe injection

Robotic automation Yes

What platform? Centri 360

Sampling make up gas N2

Syringe volume 5ml

Heat Syringe 55°C

Total sampling volume 25ml

Enrich sample on cold trap Yes

Total number of injections 5

Enrichment delay 1min

Incubation before sampling Yes

Incubation time 0.5min

Incubation temperature 50°C

Agitation during the incubation period No

Injector temperature 250°C

Injection Time 2min

Incubation during sampling No

GC-MS

Focusing trap Markes focusing trap

Focusing trap sorbent-packed UNITY-T12ME-2S Material emissions, C4 - C32

Desorb trap purge time 1min

Trap purge flow 40ml/min

Trap low temperature 10°C

Trap heating rate 100°C/s

Trap high (desorb) temperature 250°C

Trap desorb time 2min

Trap split Yes

Split flow 20ml/min

Column type DB-WAX-UI

Column flow 1.29ml/min

Pressure 14psi

Length 30m

Inner diameter 0.25mm

Film thickness 0.5μm

Carrier gas He

Temperature ramps

Number of ramps 1

GC initial temperature 35°C

GC initial temperature hold time 1min

GC first temperature ramp rate 10°C/min

GC final temperature 220°C

GC final temperature hold time 1 min

Mass Spectrometer detectors BenchTOF2 (SepSolve)

Filament Voltage 1.6V

Scan mass range 35-300

Data rate 8Hz

Ionisation -70eV

Salami

doi:10.17617/3.IC5FYO

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Tali Weiss

Weizmann Institute of Science

The department of Brain Sciences

Sample in glass vial

20ml

3.5g

Static headspace using syringe injection

Sample details

Title Salami

Collection method Sample in glass vial

Collection volume 20ml

Did not weight No

Mass of object sample 3.5g

Sample storage before sampling? Yes

Sample storage temperature before sampling 25°C

Sample storage time before sampling 0.3Hours

Sampling method

Sampling method Static headspace using syringe injection

Robotic automation Yes

What platform? Centri 360

Sampling make up gas N2

Syringe volume 5ml

Heat Syringe 55°C

Total sampling volume 25ml

Enrich sample on cold trap Yes

Total number of injections 5

Enrichment delay 1min

Incubation before sampling Yes

Incubation time 0.5min

Incubation temperature 50°C

Agitation during the incubation period Yes

Injector temperature 250°C

Injection Time 2min

Incubation during sampling No

GC-MS

Focusing trap Markes focusing trap

Focusing trap sorbent-packed UNITY-T12ME-2S Material emissions, C4 - C32

Desorb trap purge time 1min

Trap purge flow 40ml/min

Trap low temperature 10°C

Trap heating rate 100°C/s

Trap high (desorb) temperature 250°C

Trap desorb time 2min

Trap split Yes

Split flow 40ml/min

Column type DB-WAX-UI

Column flow 1.29ml/min

Pressure 14psi

Length 30m

Inner diameter 0.25mm

Film thickness 0.5μm

Carrier gas He

Temperature ramps

Number of ramps 1

GC initial temperature 35°C

GC initial temperature hold time 1min

GC first temperature ramp rate 10°C/min

GC final temperature 220°C

GC final temperature hold time 1 min

Mass Spectrometer detectors BenchTOF2 (SepSolve)

Filament Voltage 1.6V

Scan mass range 35-300

Data rate 8Hz

Ionisation -70eV

Black Pepper

doi:10.17617/3.IGDD44

Download

Tali Weiss

Weizmann Institute of Science

The department of Brain Sciences

Sample in glass vial

20ml

0.04g

Static headspace using syringe injection

Sample details

Title Black Pepper

Collection method Sample in glass vial

Collection volume 20ml

Did not weight No

Mass of object sample 0.04g

Sample storage before sampling? No

Sampling method

Sampling method Static headspace using syringe injection

Robotic automation Yes

What platform? Centri 360

Sampling make up gas N2

Syringe volume 5ml

Heat Syringe 55°C

Total sampling volume 5ml

Enrich sample on cold trap No

Incubation before sampling Yes

Incubation time 0.5min

Incubation temperature 50°C

Agitation during the incubation period Yes

Injector temperature 250°C

Injection Time 2min

Incubation during sampling No

GC-MS

Focusing trap Markes focusing trap

Focusing trap sorbent-packed UNITY-T12ME-2S Material emissions, C4 - C32

Desorb trap purge time 1min

Trap purge flow 40ml/min

Trap low temperature 10°C

Trap heating rate 100°C/s

Trap high (desorb) temperature 250°C

Trap desorb time 2min

Trap split Yes

Split flow 30ml/min

Column type DB-WAX-UI

Column flow 1.29ml/min

Pressure 14psi

Length 30m

Inner diameter 0.25mm

Film thickness 0.5μm

Carrier gas He

Temperature ramps

Number of ramps 1

GC initial temperature 35°C

GC initial temperature hold time 1min

GC first temperature ramp rate 10°C/min

GC final temperature 220°C

GC final temperature hold time 1 min

Mass Spectrometer detectors BenchTOF2 (SepSolve)

Filament Voltage 1.6V

Scan mass range 35-300

Data rate 8Hz

Ionisation -70eV

Chewing gum (bazzoca flavor)

doi:10.17617/3.BGK0TN

Download

Tali Weiss

Weizmann Institute of Science

Department of Brain Sciences

Sample in glass vial

20ml

1.4g

Static headspace using syringe injection

Sample details

Title Chewing gum (bazzoca flavor)

Collection method Sample in glass vial

Collection volume 20ml

Did not weight No

Mass of object sample 1.4g

Sample storage before sampling? No

Sampling method

Sampling method Static headspace using syringe injection

Robotic automation Yes

What platform? Centri 360

Sampling make up gas N2

Syringe volume 5ml

Heat Syringe 45°C

Total sampling volume 3ml

Enrich sample on cold trap No

Incubation before sampling Yes

Incubation time 0.5min

Incubation temperature 40°C

Agitation during the incubation period No

Injector temperature 250°C

Injection Time 2min

Incubation during sampling No

GC-MS

Focusing trap Markes focusing trap

Focusing trap sorbent-packed UNITY-T12ME-2S Material emissions, C4 - C32

Desorb trap purge time 0.5min

Trap purge flow 40ml/min

Trap low temperature 10°C

Trap heating rate 100°C/s

Trap high (desorb) temperature 250°C

Trap desorb time 2min

Trap split Yes

Split flow 40ml/min

Column type DB-WAX-UI

Column flow 1.29ml/min

Pressure 14psi

Length 30m

Inner diameter 0.25mm

Film thickness 0.5μm

Carrier gas He

Temperature ramps

Number of ramps 1

GC initial temperature 35°C

GC initial temperature hold time 1min

GC first temperature ramp rate 10°C/min

GC final temperature 220°C

GC final temperature hold time 1 min

Mass Spectrometer detectors BenchTOF2 (SepSolve)

Filament Voltage 1.6V

Scan mass range 30-300

Data rate 8Hz

Ionisation -70eV

Chives (Allium Schoenoprasum)

doi:10.17617/3.IIHW6N

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Tali Weiss

Weizmann Institute of Science

Department of Brain Sciences

Sample in glass vial

20ml

0.2g

Static headspace using syringe injection

Sample details

Title Chives (Allium Schoenoprasum)

Collection method Sample in glass vial

Collection volume 20ml

Did not weight No

Mass of object sample 0.2g

Sample storage before sampling? Yes

Sample storage temperature before sampling 25°C

Sample storage time before sampling 0.2Hours

Sampling method

Sampling method Static headspace using syringe injection

Robotic automation Yes

What platform? Centri 360

Sampling make up gas N2

Syringe volume 5ml

Heat Syringe 40°C

Total sampling volume 3ml

Enrich sample on cold trap No

Incubation before sampling No

Injector temperature 250°C

Injection Time 2min

Incubation during sampling No

GC-MS

Focusing trap Markes focusing trap

Focusing trap sorbent-packed UNITY-T12ME-2S Material emissions, C4 - C32

Desorb trap purge time 1min

Trap purge flow 40ml/min

Trap low temperature 10°C

Trap heating rate 100°C/s

Trap high (desorb) temperature 250°C

Trap desorb time 2min

Trap split Yes

Split flow 50ml/min

Column type DB-WAX-UI

Column flow 1.29ml/min

Pressure 14psi

Length 30m

Inner diameter 0.25mm

Film thickness 0.5μm

Carrier gas He

Temperature ramps

Number of ramps 1

GC initial temperature 35°C

GC initial temperature hold time 1min

GC first temperature ramp rate 10°C/min

GC final temperature 220°C

GC final temperature hold time 1 min

Mass Spectrometer detectors BenchTOF2 (SepSolve)

Filament Voltage 1.6V

Scan mass range 35-300

Data rate 8Hz

Ionisation -70eV