Title Aircraft - inside and surrounding

Project IDF paratroopers

Date of collection 2019-08-07

Collection volume (of the vial) 20ml

Did not weight Yes

Sample storage before sampling? Yes

Sample storage temperature before sampling -80°C

Sample storage time before sampling 5256Hours

Increase headspace sensitivity (“salting out”) No

Sampling method Vacuum- assisted sorbent sampling

Number of sorbents 2

1

Sorbent type Tenax TA

Mesh size 35/60

2

Sorbent type Carbopack X

Sorbent tubes length for TD 60mm

Split flow 20ml/min

Temperature ramps

Number of ramps 1

GC initial temperature 35°C  

GC initial temperature hold time 5min

GC first temperature ramp rate 15°C/min

GC final temperature 320°C

GC final temperature hold time 9 min

Title Honey

Project Predicting perception of naturalistic odors

Date of collection 2024-11-24

Collection volume (of the vial) 20ml

Did not weight No

Mass of object sample 6g

Sample storage before sampling? No

Sampling method Dynamic headspace

Number of sorbents 1

1

Sorbent type Carbopack C

Mesh size 60/80

Sorbent tubes length for TD 60mm

Sorbent tube sampling volume 30ml

Sorbent tube sampling flow rate 10ml/min

Incubation before sampling Yes

Incubation time 1min

Incubation temperature 60°C

Agitation during the incubation period Yes

Sorbent tubes storage after sampling No

Incubation during sampling Yes

Incubation temperature during sampling 55°C

Split flow 5ml/min

Temperature ramps

Number of ramps 1

GC initial temperature 40°C  

GC initial temperature hold time 1min

GC first temperature ramp rate 8°C/min

GC final temperature 240°C

GC final temperature hold time 1 min

Title Honey

Project Predicting perception of naturalistic odors

Date of collection 2025-01-15

Collection volume (of the vial) 20ml

Did not weight Yes

Sample storage before sampling? No

Sampling method Static headspace using syringe injection

Incubation before sampling Yes

Incubation time 2min

Incubation temperature 50°C

Agitation during the incubation period Yes

Enrich sample on cold trap Yes

Total number of injections 4

Enrichment delay 1min

Incubation during sampling No

Split flow 5ml/min

Temperature ramps

Number of ramps 1

GC initial temperature 35°C  

GC initial temperature hold time 1.5min

GC first temperature ramp rate 5°C/min

GC final temperature 140°C

GC final temperature hold time 1 min

Title Honey

Project Predicting perception of naturalistic odors

Date of collection 2025-09-14

Collection volume (of the vial) 20ml

Did not weight Yes

Sample storage before sampling? No

Sampling method Vacuum- assisted sorbent sampling

Number of sorbents 2

1

Sorbent type Tenax GR

Sorbent amount 100

Mesh size 35/60

2

Sorbent type Carbograph 5TD

Sorbent amount 100

Mesh size 40/60

Sorbent tubes length for TD 89mm

Split flow 30ml/min

Temperature ramps

Number of ramps 1

GC initial temperature 35°C  

GC initial temperature hold time 1min

GC first temperature ramp rate 10°C/min

GC final temperature 220°C

GC final temperature hold time 1 min

Title Coleus caninus leaves

Project Predicting perception of naturalistic odors

Date of collection 2024-11-13

Collection volume (of the vial) 20ml

Did not weight Yes

Sample storage before sampling? No

Suppressing enzyme-driven changes No

Increase headspace sensitivity (“salting out”) No

Sampling method Dynamic headspace

Number of sorbents 1

1

Sorbent type Carbopack C

Mesh size 60/80

Sorbent tubes length for TD 60mm

Sorbent tube sampling volume 10ml

Sorbent tube sampling flow rate 8ml/min

Incubation before sampling Yes

Incubation time 1min

Incubation temperature 35°C

Agitation during the incubation period Yes

Sorbent tubes storage after sampling No

Incubation during sampling Yes

Incubation temperature during sampling 30°C

Split flow 80ml/min

Temperature ramps

Number of ramps 1

GC initial temperature 40°C  

GC initial temperature hold time 1min

GC first temperature ramp rate 8°C/min

GC final temperature 240°C

GC final temperature hold time 1 min

Title Black Pepper

Project Predicting perception of naturalistic odors

Date of collection 2024-10-29

Collection volume (of the vial) 20ml

Did not weight Yes

Sample storage before sampling? No

Increase headspace sensitivity (“salting out”) No

Sampling method Dynamic headspace

Number of sorbents 1

1

Sorbent type Carbopack C

Mesh size 60/80

Sorbent tubes length for TD 60mm

Sorbent tube sampling volume 30ml

Sorbent tube sampling flow rate 10ml/min

Incubation before sampling Yes

Incubation time 1min

Incubation temperature 60°C

Agitation during the incubation period Yes

Sorbent tubes storage after sampling No

Incubation during sampling Yes

Incubation temperature during sampling 55°C

Split flow 10ml/min

Temperature ramps

Number of ramps 1

GC initial temperature 40°C  

GC initial temperature hold time 1min

GC first temperature ramp rate 8°C/min

GC final temperature 240°C

GC final temperature hold time 1 min

Title Mustard paste

Project Predicting perception of naturalistic odors

Date of collection 2024-10-29

Collection volume (of the vial) 20ml

Did not weight Yes

Sample storage before sampling? No

Increase headspace sensitivity (“salting out”) No

Sampling method Dynamic headspace

Number of sorbents 1

1

Sorbent type Carbopack C

Mesh size 60/80

Sorbent tubes length for TD 60mm

Sorbent tube sampling volume 50ml

Sorbent tube sampling flow rate 10ml/min

Incubation before sampling Yes

Incubation time 1min

Incubation temperature 60°C

Agitation during the incubation period Yes

Sorbent tubes storage after sampling No

Incubation during sampling Yes

Incubation temperature during sampling 55°C

Split flow 5ml/min

Temperature ramps

Number of ramps 1

GC initial temperature 40°C  

GC initial temperature hold time 1min

GC first temperature ramp rate 8°C/min

GC final temperature 240°C

GC final temperature hold time 1 min

Title Mustard paste

Project Predicting perception of naturalistic odors

Date of collection 2024-10-29

Collection volume (of the vial) 20ml

Did not weight Yes

Sample storage before sampling? No

Increase headspace sensitivity (“salting out”) No

Sampling method Dynamic headspace

Number of sorbents 1

1

Sorbent type TenaxTA

Mesh size 60/80

Sorbent tubes length for TD 60mm

Sorbent tube sampling volume 80ml

Sorbent tube sampling flow rate 8ml/min

Incubation before sampling Yes

Incubation time 1min

Incubation temperature 45°C

Agitation during the incubation period Yes

Sorbent tubes storage after sampling No

Incubation during sampling Yes

Incubation temperature during sampling 40°C

Split flow 5ml/min

Temperature ramps

Number of ramps 1

GC initial temperature 30°C  

GC initial temperature hold time 0.5min

GC first temperature ramp rate 10°C/min

GC final temperature 240°C

GC final temperature hold time 1 min

Title Mango rotten

Project Predicting perception of naturalistic odors

Date of collection 2024-10-26

Collection volume (of the vial) 20ml

Did not weight Yes

Sample storage before sampling? No

Suppressing enzyme-driven changes No

Increase headspace sensitivity (“salting out”) No

Sampling method Dynamic headspace

Number of sorbents 3

1

Sorbent type Carbopack C

Mesh size 60/80

2

Sorbent type Carbopack B

Mesh size 60/80

3

Sorbent type Carbosieve SIII

Mesh size 60/80

Sorbent tubes length for TD 60mm

Sorbent tube sampling volume 40ml

Sorbent tube sampling flow rate 8ml/min

Incubation before sampling Yes

Incubation time 1min

Incubation temperature 50°C

Agitation during the incubation period Yes

Sorbent tubes storage after sampling No

Incubation during sampling Yes

Incubation temperature during sampling 45°C

Split flow 30ml/min

Temperature ramps

Number of ramps 1

GC initial temperature 30°C  

GC initial temperature hold time 0.5min

GC first temperature ramp rate 5°C/min

GC final temperature 220°C

GC final temperature hold time 1 min

Title Green Onion

Project Predicting perception of naturalistic odors

Date of collection 2024-10-31

Collection volume (of the vial) 20ml

Did not weight Yes

Sample storage before sampling? No

Suppressing enzyme-driven changes No

Increase headspace sensitivity (“salting out”) No

Sampling method Dynamic headspace

Number of sorbents 1

1

Sorbent type Tenax TA

Mesh size 60/80

Sorbent tubes length for TD 60mm

Sorbent tube sampling volume 10ml

Sorbent tube sampling flow rate 8ml/min

Incubation before sampling Yes

Incubation time 1min

Incubation temperature 35°C

Agitation during the incubation period Yes

Sorbent tubes storage after sampling No

Incubation during sampling Yes

Incubation temperature during sampling 30°C

Split flow 50ml/min

Temperature ramps

Number of ramps 1

GC initial temperature 30°C  

GC initial temperature hold time 0.5min

GC first temperature ramp rate 5°C/min

GC final temperature 200°C

GC final temperature hold time 1 min