Title Pears

Date of collection 2025-01-16

Collection volume (of the vial) 20ml

Did not weight No

Mass of object sample 2g

Sample storage before sampling? No

Salts Sodium chloride

Incubation duration 1sec

Incubation temperature 25°C

Sampling method Solid-Phase Microextraction (SPME)

Extraction mode Yes

Extraction time 30min

Extraction temperature 40°C

Temperature ramps

Number of ramps 2

GC initial temperature 40°C  

GC initial temperature hold time 1min

GC first temperature ramp rate 5°C/min

GC second temperature 160°C

GC second temperature hold time 2min

GC second temperature ramp rate 10°C/min

GC final temperature 250°C

GC final temperature hold time 1 min

Title Nectarines

Date of collection 2025-06-26

Collection volume (of the vial) 20ml

Did not weight No

Mass of object sample 2g

Sample storage before sampling? No

Salts Sodium chloride

Incubation duration 1sec

Incubation temperature 25°C

Sampling method Solid-Phase Microextraction (SPME)

Extraction mode Yes

Extraction time 30min

Extraction temperature 40°C

Temperature ramps

Number of ramps 2

GC initial temperature 40°C  

GC initial temperature hold time 1min

GC first temperature ramp rate 5°C/min

GC second temperature 160°C

GC second temperature hold time 2min

GC second temperature ramp rate 10°C/min

GC final temperature 250°C

GC final temperature hold time 1 min

Title Blackberry

Date of collection 2024-06-17

Collection volume (of the vial) 20ml

Did not weight No

Mass of object sample 2g

Sample storage before sampling? No

Salts Sodium chloride

Incubation duration 2sec

Incubation temperature 25°C

Sampling method Solid-Phase Microextraction (SPME)

Extraction mode Yes

Extraction time 30min

Extraction temperature 40°C

Temperature ramps

Number of ramps 2

GC initial temperature 40°C  

GC initial temperature hold time 1min

GC first temperature ramp rate 5°C/min

GC second temperature 160°C

GC second temperature hold time 2min

GC second temperature ramp rate 10°C/min

GC final temperature 250°C

GC final temperature hold time 1 min

Title Apricot

Date of collection 2024-11-13

Collection volume (of the vial) 20ml

Did not weight No

Mass of object sample 2g

Sample storage before sampling? No

Salts Sodium chloride

Incubation duration 1sec

Incubation temperature 25°C

Sampling method Solid-Phase Microextraction (SPME)

Extraction mode Yes

Extraction time 30min

Extraction temperature 40°C

Temperature ramps

Number of ramps 2

GC initial temperature 40°C  

GC initial temperature hold time 1min

GC first temperature ramp rate 5°C/min

GC second temperature 160°C

GC second temperature hold time 2min

GC second temperature ramp rate 10°C/min

GC final temperature 250°C

GC final temperature hold time 1 min

Title Apple - Pink Lady

Date of collection 2024-08-08

Collection volume (of the vial) 20ml

Did not weight No

Mass of object sample 2g

Sample storage before sampling? No

Salts Sodium chloride

Incubation duration 1sec

Incubation temperature 25°C

Sampling method Solid-Phase Microextraction (SPME)

Extraction mode Yes

Extraction time 30min

Extraction temperature 40°C

Temperature ramps

Number of ramps 2

GC initial temperature 40°C  

GC initial temperature hold time 1min

GC first temperature ramp rate 5°C/min

GC second temperature 160°C

GC second temperature hold time 2min

GC second temperature ramp rate 10°C/min

GC final temperature 250°C

GC final temperature hold time 1 min

Title Apple - Granny Smith

Date of collection 2024-08-08

Collection volume (of the vial) 20ml

Did not weight No

Mass of object sample 2g

Sample storage before sampling? No

Salts Sodium chloride

Incubation duration 1sec

Incubation temperature 25°C

Sampling method Solid-Phase Microextraction (SPME)

Extraction mode Yes

Extraction time 30min

Extraction temperature 40°C

Temperature ramps

Number of ramps 2

GC initial temperature 40°C  

GC initial temperature hold time 1min

GC second temperature 160°C

GC second temperature hold time 2min

GC second temperature ramp rate 10°C/min

GC final temperature 250°C

GC final temperature hold time 1 min

Title Apple - Golden Delicious

Date of collection 2024-08-08

Collection volume (of the vial) 20ml

Did not weight No

Mass of object sample 2g

Sample storage before sampling? No

Salts Sodium chloride

Incubation duration 1sec

Incubation temperature 25°C

Sampling method Solid-Phase Microextraction (SPME)

Extraction mode Yes

Extraction time 30min

Extraction temperature 40°C

Temperature ramps

Number of ramps 2

GC initial temperature 40°C  

GC initial temperature hold time 1min

GC first temperature ramp rate 5°C/min

GC second temperature 160°C

GC second temperature hold time 2min

GC second temperature ramp rate 10°C/min

GC final temperature 250°C

GC final temperature hold time 1 min

Title Pecan_Delmas

Date of collection 2026-01-05

Collection volume (of the vial) 20ml

Did not weight No

Mass of object sample 2g

Sample storage before sampling? No

Salts Sodium chloride

Incubation duration 1sec

Incubation temperature 25°C

Sampling method Solid-Phase Microextraction (SPME)

Extraction mode Yes

Extraction time 30min

Extraction temperature 40°C

Temperature ramps

Number of ramps 3

GC initial temperature 40°C  

GC initial temperature hold time 2min

GC second temperature 100°C

GC second temperature ramp rate 4°C/min

GC third temperature 250°C

GC third temperature hold time 5min

GC third temperature ramp rate 10°C/min

GC final temperature 250°C

GC final temperature hold time 5 min

Title Pecan_Ha Tiv

Date of collection 2026-01-05

Collection volume (of the vial) 20ml

Did not weight No

Mass of object sample 2g

Sample storage before sampling? No

Salts Sodium chloride

Incubation duration 1sec

Incubation temperature 25°C

Sampling method Solid-Phase Microextraction (SPME)

Extraction mode Yes

Extraction time 30min

Extraction temperature 40°C

Temperature ramps

Number of ramps 3

GC initial temperature 40°C  

GC initial temperature hold time 2min

GC second temperature 100°C

GC second temperature ramp rate 4°C/min

GC third temperature 250°C

GC third temperature hold time 5min

GC third temperature ramp rate 10°C/min

GC final temperature 250°C

GC final temperature hold time 5 min

Title Pecan_Kliyat Gat

Date of collection 2026-01-05

Collection volume (of the vial) 20ml

Did not weight No

Mass of object sample 2g

Sample storage before sampling? No

Salts Sodium chloride

Incubation duration 1sec

Incubation temperature 25°C

Sampling method Solid-Phase Microextraction (SPME)

Extraction mode Yes

Extraction time 30min

Extraction temperature 40°C

Temperature ramps

Number of ramps 3

GC initial temperature 40°C  

GC initial temperature hold time 2min

GC first temperature ramp rate 4°C/min

GC second temperature 100°C

GC second temperature hold time 0min

GC second temperature ramp rate 4°C/min

GC third temperature 250°C

GC third temperature ramp rate 10°C/min

GC final temperature 250°C