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Coffee concentrated

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Heather Spooner

University of Reading, Reading, Berkshire, United Kingdom

Department of Food and Nutritional Sciences

Sample in glass vial

18ml

Solid-Phase Microextraction (SPME)

Sample details

Title Coffee concentrated

Project Parosmia Project

Date of collection 2019-10-10

Collection method Sample in glass vial

Collection volume (of the vial) 18ml

Did not weight No

Mass of object sample 1g

Sample storage before sampling? No

Material state In solution

Sampling method

Sampling method Solid-Phase Microextraction (SPME)

Robotic automation No

Sorbent type triple phase DVB/Carboxen/PDMS 1 cm
DVB 50 um Carboxen 30 um PDMS 30 um

Sorbent phase thickness 30um

Headspace equilibrium temperature 55°C

Headspace equilibrium time 10min

Extraction mode Yes

Extraction time 30min

Extraction temperature 55°C

Desorption time 20min

Desorption temperature 250°C

Vortex Yes

Vortex speed 500rpm

GC-MS

Column type HP-5 5% Phenyl Methyl Siloxan

Column constant flow 0.9ml/min

Length 30m

Inner diameter 0.25mm

Film thickness 1μm

Carrier gas He

Temperature ramps

Number of ramps 1

GC initial temperature 40°C

GC initial temperature hold time 1min

GC first temperature ramp rate 4°C/min

GC final temperature 300°C

GC final temperature hold time 5 min

Mass Spectrometer detectors Quadrupole MS 5975C (Agilent)

Scan mass range 20-280

Data rate 0.69Hz

Ionisation -70eV

Kettle water

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Heather Spooner

University of Reading, Reading, Berkshire, United Kingdom

Department of Food and Nutritional Sciences

Sample in glass vial

18ml

Solid-Phase Microextraction (SPME)

Sample details

Title Kettle water

Project Parosmia Project

Date of collection 2019-10-10

Collection method Sample in glass vial

Collection volume (of the vial) 18ml

Did not weight No

Mass of object sample 1g

Sample storage before sampling? No

Material state In solution

Sampling method

Sampling method Solid-Phase Microextraction (SPME)

Robotic automation No

Sorbent type triple phase DVB/Carboxen/PDMS 1 cm
DVB 50 um Carboxen 30 um PDMS 30 um

Sorbent phase thickness 30um

Headspace equilibrium temperature 55°C

Headspace equilibrium time 10min

Extraction mode Yes

Extraction time 30min

Extraction temperature 55°C

Desorption time 20min

Desorption temperature 250°C

Vortex Yes

Vortex speed 500rpm

GC-MS

Column type HP-5 5% Phenyl Methyl Siloxan

Column constant flow 0.9ml/min

Length 30m

Inner diameter 0.25mm

Film thickness 1μm

Carrier gas He

Temperature ramps

Number of ramps 1

GC initial temperature 40°C

GC initial temperature hold time 1min

GC first temperature ramp rate 4°C/min

GC final temperature 300°C

GC final temperature hold time 5 min

Mass Spectrometer detectors Quadrupole MS 5975C (Agilent)

Scan mass range 20-280

Data rate 0.69Hz

Ionisation -70eV

Coffee weak

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Heather Spooner

University of Reading, Reading, Berkshire, United Kingdom

Department of Food and Nutritional Sciences

Sample in glass vial

18ml

Solid-Phase Microextraction (SPME)

Sample details

Title Coffee weak

Project Parosmia Project

Date of collection 2019-10-10

Collection method Sample in glass vial

Collection volume (of the vial) 18ml

Did not weight No

Mass of object sample 1g

Sample storage before sampling? No

Material state In solution

Sampling method

Sampling method Solid-Phase Microextraction (SPME)

Robotic automation No

Sorbent type triple phase DVB/Carboxen/PDMS 1 cm
DVB 50 um Carboxen 30 um PDMS 30 um

Sorbent phase thickness 30um

Headspace equilibrium temperature 55°C

Headspace equilibrium time 10min

Extraction mode Yes

Extraction time 30min

Extraction temperature 55°C

Desorption time 20min

Desorption temperature 250°C

Vortex Yes

Vortex speed 500rpm

GC-MS

Column type HP-5 5% Phenyl Methyl Siloxan

Column constant flow 0.9ml/min

Length 30m

Inner diameter 0.25mm

Film thickness 1μm

Carrier gas He

Temperature ramps

Number of ramps 1

GC initial temperature 40°C

GC initial temperature hold time 1min

GC first temperature ramp rate 4°C/min

GC final temperature 300°C

GC final temperature hold time 5 min

Mass Spectrometer detectors Quadrupole MS 5975C (Agilent)

Scan mass range 20-280

Data rate 0.69Hz

Ionisation -70eV

Coffee

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Heather Spooner

University of Reading, Reading, Berkshire, United Kingdom

Department of Food and Nutritional Sciences

Sample in glass vial

18ml

Solid-Phase Microextraction (SPME)

Sample details

Title Coffee

Project Parosmia Project

Date of collection 2020-03-01

Collection method Sample in glass vial

Collection volume (of the vial) 18ml

Did not weight No

Mass of object sample 1g

Sample storage before sampling? No

Material state In solution

Sampling method

Sampling method Solid-Phase Microextraction (SPME)

Robotic automation No

Sorbent type triple phase DVB/Carboxen/PDMS 1 cm
DVB 50 um Carboxen 30 um PDMS 30 um

Sorbent phase thickness 30um

Headspace equilibrium temperature 50°C

Headspace equilibrium time 10min

Extraction mode Yes

Extraction time 30min

Extraction temperature 50°C

Desorption time 20min

Desorption temperature 250°C

Vortex Yes

Vortex speed 500rpm

GC-MS

Column type HP-5 5% Phenyl Methyl Siloxan

Column constant flow 0.9ml/min

Length 30m

Inner diameter 0.25mm

Film thickness 1μm

Carrier gas He

Temperature ramps

Number of ramps 1

GC initial temperature 40°C

GC initial temperature hold time 5min

GC first temperature ramp rate 4°C/min

GC final temperature 250°C

GC final temperature hold time 0 min

Mass Spectrometer detectors Quadrupole MS 5975C (Agilent)

Scan mass range 20-280

Data rate 0.69Hz

Ionisation -70eV

Coffee

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Heather Spooner

University of Reading, Reading, Berkshire, United Kingdom

Department of Food and Nutritional Sciences

Sample in glass vial

18ml

Solid-Phase Microextraction (SPME)

Sample details

Title Coffee

Project Parosmia Project

Date of collection 2020-03-01

Collection method Sample in glass vial

Collection volume (of the vial) 18ml

Did not weight No

Mass of object sample 1g

Sample storage before sampling? No

Material state In solution

Sampling method

Sampling method Solid-Phase Microextraction (SPME)

Robotic automation No

Sorbent type triple phase DVB/Carboxen/PDMS 1 cm
DVB 50 um Carboxen 30 um PDMS 30 um

Sorbent phase thickness 30um

Headspace equilibrium temperature 50°C

Headspace equilibrium time 10min

Extraction mode Yes

Extraction time 30min

Extraction temperature 50°C

Desorption time 20min

Desorption temperature 250°C

Vortex Yes

Vortex speed 500rpm

GC-MS

Column type HP-5 5% Phenyl Methyl Siloxan

Column constant flow 0.9ml/min

Length 30m

Inner diameter 0.25mm

Film thickness 1μm

Carrier gas He

Temperature ramps

Number of ramps 1

GC initial temperature 40°C

GC initial temperature hold time 5min

GC first temperature ramp rate 4°C/min

GC final temperature 250°C

GC final temperature hold time 0 min

Mass Spectrometer detectors Quadrupole MS 5975C (Agilent)

Scan mass range 20-280

Data rate 0.69Hz

Ionisation -70eV

Coffee

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Heather Spooner

University of Reading, Reading, Berkshire, United Kingdom

Department of Food and Nutritional Sciences

Sample in glass vial

18ml

Solid-Phase Microextraction (SPME)

Sample details

Title Coffee

Project Parosmia Project

Date of collection 2020-03-01

Collection method Sample in glass vial

Collection volume (of the vial) 18ml

Did not weight No

Mass of object sample 1g

Sample storage before sampling? No

Material state In solution

Sampling method

Sampling method Solid-Phase Microextraction (SPME)

Robotic automation No

Sorbent type triple phase DVB/Carboxen/PDMS 1 cm
DVB 50 um Carboxen 30 um PDMS 30 um

Sorbent phase thickness 30um

Headspace equilibrium temperature 50°C

Headspace equilibrium time 10min

Extraction mode Yes

Extraction time 30min

Extraction temperature 50°C

Desorption time 20min

Desorption temperature 250°C

Vortex Yes

Vortex speed 500rpm

GC-MS

Column type HP-5 5% Phenyl Methyl Siloxan

Column constant flow 0.9ml/min

Length 30m

Inner diameter 0.25mm

Film thickness 1μm

Carrier gas He

Temperature ramps

Number of ramps 1

GC initial temperature 40°C

GC initial temperature hold time 5min

GC first temperature ramp rate 4°C/min

GC final temperature 250°C

GC final temperature hold time 0 min

Mass Spectrometer detectors Quadrupole MS 5975C (Agilent)

Scan mass range 20-280

Data rate 0.69Hz

Ionisation -70eV

Coffee

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Heather Spooner

University of Reading, Reading, Berkshire, United Kingdom

Department of Food and Nutritional Sciences

Sample in glass vial

18ml

Solid-Phase Microextraction (SPME)

Sample details

Title Coffee

Project Parosmia Project

Date of collection 2020-03-01

Collection method Sample in glass vial

Collection volume (of the vial) 18ml

Did not weight No

Mass of object sample 1g

Sample storage before sampling? No

Material state In solution

Sampling method

Sampling method Solid-Phase Microextraction (SPME)

Robotic automation No

Sorbent type triple phase DVB/Carboxen/PDMS 1 cm
DVB 50 um Carboxen 30 um PDMS 30 um

Sorbent phase thickness 30um

Headspace equilibrium temperature 50°C

Headspace equilibrium time 10min

Extraction mode Yes

Extraction time 30min

Extraction temperature 50°C

Desorption time 20min

Desorption temperature 250°C

Vortex Yes

Vortex speed 500rpm

GC-MS

Column type HP-5 5% Phenyl Methyl Siloxan

Column constant flow 0.9ml/min

Length 30m

Inner diameter 0.25mm

Film thickness 1μm

Carrier gas He

Temperature ramps

Number of ramps 1

GC initial temperature 40°C

GC initial temperature hold time 5min

GC first temperature ramp rate 4°C/min

GC final temperature 250°C

GC final temperature hold time 0 min

Mass Spectrometer detectors Quadrupole MS 5975C (Agilent)

Scan mass range 20-280

Data rate 0.69Hz

Ionisation -70eV

Cooked Bacon

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Jane K Parker

University of Reading, Reading, Berkshire, United Kingdom

Department of Food and Nutritional Sciences

Sample in glass vial

18ml

Solid-Phase Microextraction (SPME)

Sample details

Title Cooked Bacon

Project Parosmia Project

Date of collection 2020-02-18

Collection method Sample in glass vial

Collection volume (of the vial) 18ml

Did not weight No

Mass of object sample 1g

Sample storage before sampling? Yes

Sample storage temperature before sampling 4°C

Material state Chopped

Suppressing enzyme-driven changes No

Increase headspace sensitivity (“salting out”) No

Sampling method

Sampling method Solid-Phase Microextraction (SPME)

Robotic automation No

Sorbent type triple phase DVB/Carboxen/PDMS 1 cm
DVB 50 um Carboxen 30 um PDMS 30 um

Sorbent phase thickness 30um

Headspace equilibrium temperature 50°C

Headspace equilibrium time 10min

Extraction mode Yes

Extraction time 30min

Extraction temperature 50°C

Desorption time 20min

Desorption temperature 250°C

Vortex Yes

Vortex speed 500rpm

GC-MS

Column type HP-5 5% Phenyl Methyl Siloxan

Column constant flow 0.9ml/min

Length 30m

Inner diameter 0.25mm

Film thickness 1μm

Carrier gas He

Temperature ramps

Number of ramps 1

GC initial temperature 40°C

GC initial temperature hold time 5min

GC first temperature ramp rate 4°C/min

GC final temperature 250°C

GC final temperature hold time 0 min

Mass Spectrometer detectors Quadrupole MS 5975C (Agilent)

Scan mass range 20-280

Data rate 0.69Hz

Ionisation -70eV

Sheep_1

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Yael Laor

Agricultural Research Organization (ARO) – Volcani Institute

Newe Ya'ar Research Center

Outdoor source emission

Flux chamber

Sample details

Title Sheep_1

Project Odor emissions from livestock in Israel

Date of collection 2025-12-01

Citation None

Collection method Outdoor source emission

Sampling method

Sampling method Flux chamber

Number of sorbents 2

Sorbent type Tenax TA

Sorbent amount 100

Mesh size 40/60

Sorbent type Carbograph 1TD

Sorbent amount 100

Mesh size 40/60

Sorbent tubes length for TD 89mm

Sorbent tube sampling volume 2ml

Sorbent tube sampling flow rate 200ml/min

Sorbent tubes storage after sampling Yes

Time between sampling and desorption 20000min

Storage at temperature 4°C

TDU type Centri

Tube desorption stages 2

Desorb time 1min

Desorb temperature 200°C

GC-MS

Temperature ramps

Number of ramps 1

Ionisation -70eV

Otebo Bean Unroasted Flour 2023

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Faith Zillinger

Michigan State University

Department of Food Science and Human Nutrition

Sample in glass vial

20ml

Solid-Phase Microextraction (SPME)

Sample details

Title Otebo Bean Unroasted Flour 2023

Project Pulse Flours

Citation https://doi.org/10.1111/1750-3841.70608

Collection method Sample in glass vial

Collection volume (of the vial) 20ml

Did not weight No

Mass of object sample 2g

Sample storage before sampling? Yes

Sample storage temperature before sampling 2°C

Sample storage time before sampling 525600Hours

Material state Dried

Sampling method

Sampling method Solid-Phase Microextraction (SPME)

Robotic automation Yes

What platform? Gerstel MPS

Sorbent type DVB/CAR/PDMS

Sorbent phase thickness 30um

Headspace equilibrium temperature 50°C

Headspace equilibrium time 30min

Extraction mode Yes

Extraction time 30min

Extraction temperature 50°C

Desorption time 0.3min

Desorption temperature 200°C

Vortex No

GC-MS

Focusing trap Cooled Injection System

CIS low temperature -196°C

Trap split {Empty}

Column type HP-5

Column constant flow 1.8ml/min

Length 30m

Inner diameter .25mm

Film thickness .25μm

Carrier gas He

Temperature ramps

Number of ramps 3

GC initial temperature 32°C

GC initial temperature hold time .25min

GC first temperature ramp rate 20°C/min

GC second temperature 60°C

GC second temperature hold time 0.00min

GC second temperature ramp rate 50°C/min

GC third temperature 150°C

GC third temperature hold time 0.00min

GC third temperature ramp rate 70°C/min

GC final temperature 280°C

GC final temperature hold time 2 min

Mass Spectrometer detectors TOF (Leco)

Scan mass range 29-400

Data rate 20Hz

Ionisation -70eV