Title Alkane Roasted Jack Fruit Seeds DB5

Project Jack Fruit

Date of collection 2016-11-10

Citation 10.1016/j.foodchem.2021.129537

Collection volume (of the vial) 18ml

Did not weight No

Mass of object sample 2g

Sample storage before sampling? No

Increase headspace sensitivity (“salting out”) {Empty}

Sampling method Solid-Phase Microextraction (SPME)

Extraction mode Yes

Extraction time 55min

Extraction temperature 45°C

Temperature ramps

Number of ramps 1

GC initial temperature 40°C  

GC initial temperature hold time 1min

GC first temperature ramp rate 5°C/min

GC final temperature 250°C

GC final temperature hold time 0 min

Title Traditional Beechwood smoked water Filtered

Project Smoked Water: different woods

Date of collection 2022-05-26

Citation Kannokan Panchan, Thesis University of Reading 2023

Collection volume (of the vial) 18ml

Did not weight No

Mass of object sample 2g

Sample storage before sampling? No

Increase headspace sensitivity (“salting out”) {Empty}

Sampling method Solid-Phase Microextraction (SPME)

Extraction mode Yes

Extraction time 30min

Extraction temperature 60°C

Temperature ramps

Number of ramps 1

GC initial temperature 60°C  

GC initial temperature hold time 0min

GC first temperature ramp rate 6°C/min

GC final temperature 300°C

GC final temperature hold time 20 min

Title Rosmarine leaves

Project Predicting perception of naturalistic odors

Date of collection 2024-10-13

Collection volume (of the vial) 20ml

Did not weight Yes

Sample storage before sampling? No

Suppressing enzyme-driven changes No

Increase headspace sensitivity (“salting out”) No

Sampling method Dynamic headspace

Number of sorbents 2

1

Sorbent type Tenax TA

Mesh size 60/80

2

Sorbent type Carbograph 5

Mesh size 60/80

Sorbent tubes length for TD 60mm

Sorbent tube sampling volume 20ml

Sorbent tube sampling flow rate 10ml/min

Incubation before sampling Yes

Incubation time 1min

Incubation temperature 45°C

Agitation during the incubation period Yes

Sorbent tubes storage after sampling No

Incubation during sampling Yes

Incubation temperature during sampling 37°C

Split flow 100ml/min

Temperature ramps

Number of ramps 3

GC initial temperature 30°C  

GC initial temperature hold time 0.5min

GC first temperature ramp rate 12°C/min

GC second temperature 90°C

GC second temperature hold time 1min

GC second temperature ramp rate 5°C/min

GC third temperature 150°C

GC third temperature hold time 0.5min

GC third temperature ramp rate 12°C/min

GC final temperature 210°C

GC final temperature hold time 1 min

Title Mango

Project Predicting perception of naturalistic odors

Date of collection 2024-10-11

Collection volume (of the vial) 20ml

Did not weight Yes

Sample storage before sampling? No

Suppressing enzyme-driven changes No

Increase headspace sensitivity (“salting out”) No

Sampling method Dynamic headspace

Number of sorbents 3

1

Sorbent type Carbopack C

Mesh size 60/80

2

Sorbent type Carbopack B

Mesh size 60/80

3

Sorbent type Carbosieve SIII

Mesh size 60/80

Sorbent tubes length for TD 60mm

Sorbent tube sampling volume 50ml

Sorbent tube sampling flow rate 10ml/min

Incubation before sampling Yes

Incubation time 1min

Incubation temperature 40°C

Agitation during the incubation period Yes

Sorbent tubes storage after sampling No

Incubation during sampling Yes

Incubation temperature during sampling 35°C

Split flow 10ml/min

Temperature ramps

Number of ramps 3

GC initial temperature 30°C  

GC initial temperature hold time 2min

GC first temperature ramp rate 16°C/min

GC second temperature 90°C

GC second temperature hold time 1min

GC second temperature ramp rate 5°C/min

GC third temperature 140°C

GC third temperature hold time 1min

GC third temperature ramp rate 10°C/min

GC final temperature 220°C

GC final temperature hold time 1 min

Title Mango

Project Predicting perception of naturalistic odors from e-nose

Date of collection 2024-10-11

Collection volume (of the vial) 20ml

Did not weight Yes

Sample storage before sampling? No

Suppressing enzyme-driven changes No

Increase headspace sensitivity (“salting out”) No

Sampling method Dynamic headspace

Number of sorbents 1

1

Sorbent type Carbopack B

Mesh size 60/80

Sorbent tubes length for TD 60mm

Sorbent tube sampling volume 40ml

Sorbent tube sampling flow rate 8ml/min

Incubation before sampling Yes

Incubation time 1min

Incubation temperature 40°C

Agitation during the incubation period Yes

Sorbent tubes storage after sampling No

Incubation during sampling Yes

Incubation temperature during sampling 35°C

Split flow 10ml/min

Temperature ramps

Number of ramps 1

GC initial temperature 30°C  

GC initial temperature hold time 2min

GC first temperature ramp rate 10°C/min

GC final temperature 260°C

GC final temperature hold time 1 min

Title Peanut butter paste

Project Predicting perception of naturalistic odors from e-nose

Date of collection 2024-10-11

Collection volume (of the vial) 20ml

Did not weight Yes

Sample storage before sampling? No

Increase headspace sensitivity (“salting out”) No

Sampling method Dynamic headspace

Number of sorbents 3

1

Sorbent type Carbograph C

Mesh size 60/80

2

Sorbent type Carbograph B

Mesh size 60/80

3

Sorbent type Carbosieve SIII

Mesh size 60/80

Sorbent tubes length for TD 60mm

Sorbent tube sampling volume 40ml

Sorbent tube sampling flow rate 10ml/min

Incubation before sampling Yes

Incubation time 0min

Incubation temperature 40°C

Agitation during the incubation period Yes

Sorbent tubes storage after sampling No

Incubation during sampling Yes

Incubation temperature during sampling 35°C

Split flow 10ml/min

Temperature ramps

Number of ramps 1

GC initial temperature 30°C  

GC initial temperature hold time 2min

GC first temperature ramp rate 10°C/min

GC final temperature 260°C

GC final temperature hold time 1 min

Title Grass_lawn

Project Predicting perception of naturalistic odors from e-nose

Date of collection 2024-10-10

Collection volume (of the vial) 20ml

Did not weight Yes

Sample storage before sampling? No

Suppressing enzyme-driven changes No

Increase headspace sensitivity (“salting out”) No

Sampling method Dynamic headspace

Number of sorbents 3

1

Sorbent type Carbograph C

Mesh size 60/80

2

Sorbent type Carbograph B

Mesh size 60/80

3

Sorbent type Carbosieve SIII

Mesh size 60/80

Sorbent tubes length for TD 60mm

Sorbent tube sampling volume 40ml

Sorbent tube sampling flow rate 10ml/min

Incubation before sampling No

Sorbent tubes storage after sampling No

Incubation during sampling No

Split flow 10ml/min

Temperature ramps

Number of ramps 3

GC initial temperature 30°C  

GC initial temperature hold time 1min

GC first temperature ramp rate 12°C/min

GC second temperature 80°C

GC second temperature hold time 1min

GC second temperature ramp rate 5°C/min

GC third temperature 160°C

GC third temperature hold time 1min

GC third temperature ramp rate 12°C/min

GC final temperature 220°C

GC final temperature hold time 0 min

Title Grass_clover

Project Predicting perception of naturalistic odors

Date of collection 2024-10-10

Collection volume (of the vial) 20ml

Did not weight Yes

Sample storage before sampling? No

Suppressing enzyme-driven changes No

Increase headspace sensitivity (“salting out”) No

Sampling method Dynamic headspace

Number of sorbents 3

1

Sorbent type Carbograph C

Mesh size 60/80

2

Sorbent type Carbograph B

Mesh size 60/80

3

Sorbent type Carbosieve SIII

Mesh size 60/80

Sorbent tubes length for TD 60mm

Sorbent tube sampling volume 40ml

Sorbent tube sampling flow rate 10ml/min

Incubation before sampling Yes

Incubation time 1min

Incubation temperature 50°C

Agitation during the incubation period Yes

Sorbent tubes storage after sampling No

Incubation during sampling Yes

Incubation temperature during sampling 45°C

Split flow 10ml/min

Temperature ramps

Number of ramps 3

GC initial temperature 30°C  

GC initial temperature hold time 1min

GC first temperature ramp rate 12°C/min

GC second temperature 80°C

GC second temperature hold time 1min

GC second temperature ramp rate 5°C/min

GC third temperature 160°C

GC third temperature hold time 1min

GC third temperature ramp rate 12°C/min

GC final temperature 220°C

GC final temperature hold time 0 min

Title Grass_lawn

Project Predicting perception of naturalistic odors

Date of collection 2024-10-10

Collection volume (of the vial) 20ml

Did not weight Yes

Sample storage before sampling? No

Suppressing enzyme-driven changes No

Increase headspace sensitivity (“salting out”) No

Sampling method Dynamic headspace

Number of sorbents 3

1

Sorbent type Carbograph C

Mesh size 60/80

2

Sorbent type Carbograph B

Mesh size 60/80

3

Sorbent type Carbosieve SIII

Mesh size 60/80

Sorbent tubes length for TD 60mm

Sorbent tube sampling volume 40ml

Sorbent tube sampling flow rate 10ml/min

Incubation before sampling Yes

Incubation time 1min

Incubation temperature 50°C

Agitation during the incubation period Yes

Sorbent tubes storage after sampling No

Incubation during sampling Yes

Incubation temperature during sampling 45°C

Split flow 5ml/min

Temperature ramps

Number of ramps 1

GC initial temperature 30°C  

GC initial temperature hold time 2min

GC first temperature ramp rate 10°C/min

GC final temperature 240°C

GC final temperature hold time 1 min

Title Roasted Coffee Beans, Arabia

Project Predicting perception of naturalistic odors

Date of collection 2024-10-10

Collection volume (of the vial) 20ml

Did not weight No

Sample storage before sampling? No

Increase headspace sensitivity (“salting out”) No

Sampling method Dynamic headspace

Number of sorbents 1

1

Sorbent type TenaxTA

Mesh size 60/80

Sorbent tubes length for TD 60mm

Sorbent tube sampling volume 40ml

Sorbent tube sampling flow rate 10ml/min

Incubation before sampling Yes

Incubation time 1min

Incubation temperature 45°C

Agitation during the incubation period Yes

Sorbent tubes storage after sampling No

Incubation during sampling Yes

Incubation temperature during sampling 40°C

Split flow 50ml/min

Temperature ramps

Number of ramps 1

GC initial temperature 30°C  

GC initial temperature hold time 2min

GC first temperature ramp rate 10°C/min

GC final temperature 260°C

GC final temperature hold time 1 min