Home | D2SmellData

Plastic Wrapper New Bed Sheets

Download

view

Shiri Karagach Rubin

Weizmann Institute of Science

The department of Brain Sciences

Sample in glass vial

10ml

Dynamic headspace

Sample details

Title Plastic Wrapper New Bed Sheets

Date of collection 2021-11-02

Collection method Sample in glass vial

Collection volume (of the vial) 10ml

Did not weight Yes

Sample storage before sampling? No

Material state Fresh

Increase headspace sensitivity (“salting out”) No

Sampling method

Sampling method Dynamic headspace

Robotic automation Yes

What platform? Gerstel MPS

Number of sorbents 2

Sorbent type Tenax TA

Mesh size 60/80

Sorbent type Carbopack X

Mesh size 40/60

Sorbent tubes length for TD 60mm

Sorbent tube sampling volume 500ml

Sorbent tube sampling flow rate 50ml/min

Incubation before sampling No

Sorbent tubes storage after sampling No

Incubation during sampling No

Dry purge time 1min

Dry purge flow 50ml/min

TDU type Gerstle TDU2

Tube desorption stages 1

Desorb temperature 250°C

GC-MS

Focusing trap Cooled Injection System

CIS low temperature -10°C

CIS high temperature 250°C

Trap split No

Column type DB-5

Length 30m

Carrier gas He

Temperature ramps

Number of ramps 1

GC initial temperature 50°C

GC initial temperature hold time 1.5min

GC first temperature ramp rate 20°C/min

GC final temperature 300°C

GC final temperature hold time 1 min

Mass Spectrometer detectors Quadrupole-MS Agilent

Scan mass range 40-450

Data rate 1Hz

Ionisation -70eV

New Bed Sheets

Download

view

Shiri Karagach Rubin

Weizmann Institute of Science

The department of Brain Sciences

Sample in glass vial

10ml

Dynamic headspace

Sample details

Title New Bed Sheets

Date of collection 2021-11-02

Collection method Sample in glass vial

Collection volume (of the vial) 10ml

Did not weight Yes

Sample storage before sampling? No

Material state Fresh

Increase headspace sensitivity (“salting out”) No

Sampling method

Sampling method Dynamic headspace

Robotic automation Yes

What platform? Gerstel MPS

Number of sorbents 2

Sorbent type Tenax TA

Mesh size 60/80

Sorbent type Carbopack X

Mesh size 40/60

Sorbent tubes length for TD 60mm

Sorbent tube sampling volume 500ml

Sorbent tube sampling flow rate 50ml/min

Incubation before sampling No

Sorbent tubes storage after sampling No

Incubation during sampling No

Dry purge time 1min

Dry purge flow 50ml/min

TDU type Gerstle TDU2

Tube desorption stages 1

Desorb temperature 250°C

GC-MS

Focusing trap Cooled Injection System

CIS low temperature -10°C

CIS high temperature 250°C

Trap split No

Column type DB-5

Length 30m

Carrier gas He

Temperature ramps

Number of ramps 1

GC initial temperature 50°C

GC initial temperature hold time 1.5min

GC first temperature ramp rate 20°C/min

GC final temperature 300°C

GC final temperature hold time 1 min

Mass Spectrometer detectors Quadrupole-MS Agilent

Scan mass range 40-450

Data rate 1Hz

Ionisation -70eV

Alkane (syrups)

Download

view

Heather Spooner

University of Reading, England

Food and Nutritional Sciences

Sample in glass vial

18ml

Solid-Phase Microextraction (SPME)

Sample details

Title Alkane (syrups)

Project Parosmia Project

Date of collection 2022-03-21

Collection method Sample in glass vial

Collection volume (of the vial) 18ml

Did not weight No

Mass of object sample 1g

Sample storage before sampling? Yes

Sample storage temperature before sampling 4°C

Material state Diethyl ether

Increase headspace sensitivity (“salting out”) {Empty}

Sampling method

Sampling method Solid-Phase Microextraction (SPME)

Robotic automation No

Sorbent type triple phase DVB/Carboxen/PDMS 1 cm
DVB 50 um Carboxen 30 um PDMS 30 um

Sorbent phase thickness 30um

Headspace equilibrium temperature 40°C

Headspace equilibrium time 20min

Extraction mode Yes

Extraction time 20min

Extraction temperature 40°C

Desorption time 20min

Desorption temperature 250°C

Vortex Yes

Vortex speed 500rpm

GC-MS

Column type HP-5 5% Phenyl Methyl Siloxan

Column constant flow 0.9ml/min

Length 30m

Inner diameter 0.25mm

Film thickness 1μm

Carrier gas He

Temperature ramps

Number of ramps 1

GC initial temperature 40°C

GC initial temperature hold time 2min

GC first temperature ramp rate 4°C/min

GC final temperature 250°C

GC final temperature hold time 8 min

Mass Spectrometer detectors Quadrupole MS 5975C (Agilent)

Scan mass range 20-280

Data rate 0.69Hz

Ionisation -70eV

Baby Poop

Download

view

Shiri Karagach Rubin

Weizmann Institute of Science

The department of Brain Sciences

Sample in glass vial

20ml

0.058g

Dynamic headspace

Sample details

Title Baby Poop

Project Poop in babies

Date of collection 2025-01-20

Collection method Sample in glass vial

Collection volume (of the vial) 20ml

Did not weight No

Mass of object sample 0.058g

Sample storage before sampling? No

Material state Fresh

Increase headspace sensitivity (“salting out”) No

Sampling method

Sampling method Dynamic headspace

Robotic automation Yes

What platform? Gerstel MPS

Number of sorbents 2

Sorbent type Tenax GR

Sorbent type Carbopack B

Sorbent tubes length for TD 60mm

Incubation before sampling No

Sorbent tubes storage after sampling No

Incubation during sampling No

TDU type Gerstle TDU2

Tube desorption stages 1

GC-MS

Focusing trap Cooled Injection System

Trap split No

Column type DB-5

Length 30m

Carrier gas He

Temperature ramps

Number of ramps 1

GC initial temperature 30°C

GC initial temperature hold time 1min

GC first temperature ramp rate 5°C/min

GC final temperature 180°C

GC final temperature hold time 1 min

Mass Spectrometer detectors Quadrupole-MS Agilent

Scan mass range 35-200

Data rate 1Hz

Ionisation -70eV

Canned tuna (in oil)

Download

view

Tali Weiss

Weizmann Institute of Science

The department of Brain Sciences

Sample in glass vial

20ml

Static headspace using syringe injection

Sample details

Title Canned tuna (in oil)

Project Predicting perception from enose

Date of collection 2025-01-20

Collection method Sample in glass vial

Collection volume (of the vial) 20ml

Did not weight No

Mass of object sample 6g

Sample storage before sampling? No

Material state Chopped

Suppressing enzyme-driven changes No

Increase headspace sensitivity (“salting out”) No

Sampling method

Sampling method Static headspace using syringe injection

Robotic automation Yes

What platform? Centri 360

Incubation before sampling No

Syringe volume 5ml

Heat Syringe 60°C

Total sampling volume 20ml

Enrich sample on cold trap Yes

Total number of injections 4

Enrichment delay 1min

Injector temperature 200°C

Injection Time 2min

Incubation during sampling No

GC-MS

Focusing trap Markes focusing trap

Focusing trap sorbent-packed UNITY-T12ME-2S Material emissions, C4 - C32

Desorb trap purge time 3min

Trap purge flow 40ml/min

Trap low temperature 10°C

Trap heating rate 100°C/s

Trap high (desorb) temperature 220°C

Trap desorb time 3min

Trap split Yes

Split flow 20ml/min

Column type HP-5ms Ultra Inert

Column constant flow 1ml/min

Length 30m

Inner diameter 0.25mm

Film thickness 0.25μm

Carrier gas He

Temperature ramps

Number of ramps 1

GC initial temperature 30°C

GC initial temperature hold time 1min

GC first temperature ramp rate 5°C/min

GC final temperature 180°C

GC final temperature hold time 1 min

Mass Spectrometer detectors BenchTOF2 (SepSolve)

Scan mass range 35-200

Data rate 10Hz

Ionisation -70eV

Canned tuna (in oil)

Download

view

Tali Weiss

Weizmann Institute of Science

The department of Brain Sciences

Sample in glass vial

20ml

3.7g

Static headspace using syringe injection

Sample details

Title Canned tuna (in oil)

Project Predicting perception of naturalistic odors

Date of collection 2025-01-19

Collection method Sample in glass vial

Collection volume (of the vial) 20ml

Did not weight No

Mass of object sample 3.7g

Sample storage before sampling? No

Material state Chopped

Suppressing enzyme-driven changes No

Increase headspace sensitivity (“salting out”) No

Sampling method

Sampling method Static headspace using syringe injection

Robotic automation Yes

What platform? Centri 360

Incubation before sampling No

Syringe volume 5ml

Heat Syringe 50°C

Total sampling volume 10ml

Enrich sample on cold trap Yes

Total number of injections 2

Enrichment delay 1min

Injector temperature 180°C

Injection Time 2min

Incubation during sampling No

GC-MS

Focusing trap Markes focusing trap

Focusing trap sorbent-packed UNITY-T12ME-2S Material emissions, C4 - C32

Desorb trap purge time 3min

Trap purge flow 40ml/min

Trap low temperature 10°C

Trap heating rate 100°C/s

Trap high (desorb) temperature 200°C

Trap desorb time 3min

Trap split Yes

Split flow 20ml/min

Column type HP-5ms Ultra Inert

Column constant flow 1ml/min

Length 30m

Inner diameter 0.25mm

Film thickness 0.25μm

Carrier gas He

Temperature ramps

Number of ramps 1

GC initial temperature 35°C

GC initial temperature hold time 1.5min

GC first temperature ramp rate 5°C/min

GC final temperature 140°C

GC final temperature hold time 1 min

Mass Spectrometer detectors BenchTOF2 (SepSolve)

Scan mass range 35-200

Data rate 10Hz

Ionisation -70eV

Vanilla syrup

Download

view

Heather Spooner

University of Reading, Reading, Berkshire, United Kingdom

Department of Food and Nutritional Sciences

Sample in glass vial

18ml

Solid-Phase Microextraction (SPME)

Sample details

Title Vanilla syrup

Project Parosmia Project

Date of collection 2022-03-21

Collection method Sample in glass vial

Collection volume (of the vial) 18ml

Did not weight No

Mass of object sample 1g

Sample storage before sampling? Yes

Sample storage temperature before sampling 4°C

Material state syrup

Increase headspace sensitivity (“salting out”) {Empty}

Sampling method

Sampling method Solid-Phase Microextraction (SPME)

Robotic automation No

Sorbent type triple phase DVB/Carboxen/PDMS 1 cm
DVB 50 um Carboxen 30 um PDMS 30 um

Sorbent phase thickness 30um

Headspace equilibrium temperature 40°C

Headspace equilibrium time 20min

Extraction mode Yes

Extraction time 20min

Extraction temperature 40°C

Desorption time 20min

Desorption temperature 250°C

Vortex Yes

Vortex speed 500rpm

GC-MS

Column type HP-5 5% Phenyl Methyl Siloxan

Column constant flow 0.9ml/min

Length 30m

Inner diameter 0.25mm

Film thickness 1μm

Carrier gas He

Temperature ramps

Number of ramps 1

GC initial temperature 40°C

GC initial temperature hold time 2min

GC first temperature ramp rate 4°C/min

GC final temperature 250°C

GC final temperature hold time 8 min

Mass Spectrometer detectors Quadrupole MS 5975C (Agilent)

Scan mass range 20-280

Data rate 0.69Hz

Ionisation -70eV

Hazelnut syrup

Download

view

Heather Spooner

University of Reading, Reading, Berkshire, United Kingdom

Department of Food and Nutritional Sciences

Sample in glass vial

18ml

Solid-Phase Microextraction (SPME)

Sample details

Title Hazelnut syrup

Project Parosmia Project

Date of collection 2022-03-21

Collection method Sample in glass vial

Collection volume (of the vial) 18ml

Did not weight No

Mass of object sample 1g

Sample storage before sampling? Yes

Sample storage temperature before sampling 4°C

Material state syrup

Increase headspace sensitivity (“salting out”) {Empty}

Sampling method

Sampling method Solid-Phase Microextraction (SPME)

Robotic automation No

Sorbent type triple phase DVB/Carboxen/PDMS 1 cm
DVB 50 um Carboxen 30 um PDMS 30 um

Sorbent phase thickness 30um

Headspace equilibrium temperature 40°C

Headspace equilibrium time 20min

Extraction mode Yes

Extraction time 20min

Extraction temperature 40°C

Desorption time 20min

Desorption temperature 250°C

Vortex Yes

Vortex speed 500rpm

GC-MS

Column type HP-5 5% Phenyl Methyl Siloxan

Column constant flow 0.9ml/min

Length 30m

Inner diameter 0.25mm

Film thickness 1μm

Carrier gas He

Temperature ramps

Number of ramps 1

GC initial temperature 40°C

GC initial temperature hold time 2min

GC first temperature ramp rate 4°C/min

GC final temperature 250°C

GC final temperature hold time 8 min

Mass Spectrometer detectors Quadrupole MS 5975C (Agilent)

Scan mass range 20-280

Data rate 0.69Hz

Ionisation -70eV

Gingerbread syrup

Download

view

Heather Spooner

University of Reading, Reading, Berkshire, United Kingdom

Department of Food and Nutritional Sciences

Sample in glass vial

18ml

Solid-Phase Microextraction (SPME)

Sample details

Title Gingerbread syrup

Project Parosmia Project

Date of collection 2022-03-21

Collection method Sample in glass vial

Collection volume (of the vial) 18ml

Did not weight No

Mass of object sample 1g

Sample storage before sampling? Yes

Sample storage temperature before sampling 4°C

Material state syrup

Increase headspace sensitivity (“salting out”) {Empty}

Sampling method

Sampling method Solid-Phase Microextraction (SPME)

Robotic automation No

Sorbent type triple phase DVB/Carboxen/PDMS 1 cm
DVB 50 um Carboxen 30 um PDMS 30 um

Sorbent phase thickness 30um

Headspace equilibrium temperature 40°C

Headspace equilibrium time 20min

Extraction mode Yes

Extraction time 20min

Extraction temperature 40°C

Desorption time 20min

Desorption temperature 250°C

Vortex Yes

Vortex speed 500rpm

GC-MS

Column type HP-5 5% Phenyl Methyl Siloxan

Column constant flow 0.9ml/min

Length 30m

Inner diameter 0.25mm

Film thickness 1μm

Carrier gas He

Temperature ramps

Number of ramps 1

GC initial temperature 40°C

GC initial temperature hold time 2min

GC first temperature ramp rate 4°C/min

GC final temperature 250°C

GC final temperature hold time 8 min

Mass Spectrometer detectors Quadrupole MS 5975C (Agilent)

Scan mass range 20-280

Data rate 0.69Hz

Ionisation -70eV

Caramel syrup

Download

view

Heather Spooner

University of Reading, Reading, Berkshire, United Kingdom

Department of Food and Nutritional Sciences

Sample in glass vial

18ml

Solid-Phase Microextraction (SPME)

Sample details

Title Caramel syrup

Project Parosmia Project

Date of collection 2022-03-21

Collection method Sample in glass vial

Collection volume (of the vial) 18ml

Did not weight No

Mass of object sample 1g

Sample storage before sampling? Yes

Sample storage temperature before sampling 4°C

Material state syrup

Increase headspace sensitivity (“salting out”) {Empty}

Sampling method

Sampling method Solid-Phase Microextraction (SPME)

Robotic automation No

Sorbent type triple phase DVB/Carboxen/PDMS 1 cm
DVB 50 um Carboxen 30 um PDMS 30 um

Sorbent phase thickness 30um

Headspace equilibrium temperature 40°C

Headspace equilibrium time 20min

Extraction mode Yes

Extraction time 20min

Extraction temperature 40°C

Desorption time 20min

Desorption temperature 250°C

Vortex Yes

Vortex speed 500rpm

GC-MS

Column type HP-5 5% Phenyl Methyl Siloxan

Column constant flow 0.9ml/min

Length 30m

Inner diameter 0.25mm

Film thickness 1μm

Carrier gas He

Temperature ramps

Number of ramps 1

GC initial temperature 40°C

GC initial temperature hold time 2min

GC first temperature ramp rate 4°C/min

GC final temperature 250°C

GC final temperature hold time 8 min

Mass Spectrometer detectors Quadrupole MS 5975C (Agilent)

Scan mass range 20-280

Data rate 0.69Hz

Ionisation -70eV