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Otebo Bean Unroasted Flour 2022

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Faith Zillinger

Michigan State University

Department of Food Science and Human Nutrition

Sample in glass vial

20ml

Solid-Phase Microextraction (SPME)

Sample details

Title Otebo Bean Unroasted Flour 2022

Project Pulse Flours

Citation https://doi.org/10.1111/1750-3841.70608

Collection method Sample in glass vial

Collection volume (of the vial) 20ml

Did not weight No

Mass of object sample 2g

Sample storage before sampling? Yes

Sample storage temperature before sampling 2°C

Sample storage time before sampling 13140Hours

Material state Dried

Sampling method

Sampling method Solid-Phase Microextraction (SPME)

Robotic automation Yes

What platform? Gerstel MPS

Sorbent type DVB/CAR/PDMS

Sorbent phase thickness 30um

Headspace equilibrium temperature 50°C

Headspace equilibrium time 30min

Extraction mode Yes

Extraction time 30min

Extraction temperature 50°C

Desorption time 0.3min

Desorption temperature 200°C

Vortex No

GC-MS

Focusing trap Cooled Injection System

CIS low temperature -196°C

Trap split {Empty}

Column type HP-5

Column constant flow 1.8ml/min

Length 30m

Inner diameter .25mm

Film thickness .25μm

Carrier gas He

Temperature ramps

Number of ramps 3

GC initial temperature 32°C

GC initial temperature hold time .25min

GC first temperature ramp rate 20°C/min

GC second temperature 60°C

GC second temperature hold time 0.00min

GC second temperature ramp rate 50°C/min

GC third temperature 150°C

GC third temperature hold time 0.00min

GC third temperature ramp rate 70°C/min

GC final temperature 280°C

GC final temperature hold time 2 min

Mass Spectrometer detectors TOF (Leco)

Scan mass range 29-400

Data rate 20Hz

Ionisation -70eV

Otebo Bean Roasted Flour 2022

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Faith Zillinger

Michigan State University

Department of Food Science and Human Nutrition

Sample in glass vial

20ml

Solid-Phase Microextraction (SPME)

Sample details

Title Otebo Bean Roasted Flour 2022

Project Pulse Flours

Citation https://doi.org/10.1111/1750-3841.70608

Collection method Sample in glass vial

Collection volume (of the vial) 20ml

Did not weight No

Mass of object sample 2g

Sample storage before sampling? Yes

Sample storage temperature before sampling 2°C

Sample storage time before sampling 13140Hours

Material state Dried

Sampling method

Sampling method Solid-Phase Microextraction (SPME)

Robotic automation Yes

What platform? Gerstel MPS

Sorbent type DVB/CAR/PDMS

Sorbent phase thickness 30um

Headspace equilibrium temperature 50°C

Headspace equilibrium time 30min

Extraction mode Yes

Extraction time 30min

Extraction temperature 50°C

Desorption time 0.3min

Desorption temperature 200°C

Vortex No

GC-MS

Focusing trap Cooled Injection System

CIS low temperature -196°C

Trap split {Empty}

Column type HP-5

Column constant flow 1.8ml/min

Length 30m

Inner diameter .25mm

Film thickness .25μm

Carrier gas He

Temperature ramps

Number of ramps 3

GC initial temperature 32°C

GC initial temperature hold time .25min

GC first temperature ramp rate 20°C/min

GC second temperature 60°C

GC second temperature hold time 0.00min

GC second temperature ramp rate 50°C/min

GC third temperature 150°C

GC third temperature hold time 0.00min

GC third temperature ramp rate 70°C/min

GC final temperature 280°C

GC final temperature hold time 2 min

Mass Spectrometer detectors TOF (Leco)

Scan mass range 29-400

Data rate 20Hz

Ionisation -70eV

Chickpea Unroasted Porridge 2022

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Faith Zillinger

Michigan State University

Department of Food Science and Human Nutrition

Sample in glass vial

20ml

Solid-Phase Microextraction (SPME)

Sample details

Title Chickpea Unroasted Porridge 2022

Project Pulse Flours

Citation https://doi.org/10.1111/1750-3841.70608

Collection method Sample in glass vial

Collection volume (of the vial) 20ml

Did not weight No

Mass of object sample 5g

Sample storage before sampling? No

Material state Fresh, Crushed

Suppressing enzyme-driven changes No

Increase headspace sensitivity (“salting out”) Yes

Salts Sodium chloride

Sampling method

Sampling method Solid-Phase Microextraction (SPME)

Robotic automation Yes

What platform? Gerstel MPS

Sorbent type DVB/CAR/PDMS

Sorbent phase thickness 30um

Headspace equilibrium temperature 50°C

Headspace equilibrium time 30min

Extraction mode Yes

Extraction time 30min

Extraction temperature 50°C

Desorption time 0.3min

Desorption temperature 200°C

Vortex No

GC-MS

Focusing trap Cooled Injection System

CIS low temperature -196°C

Trap split {Empty}

Column type HP-5

Column constant flow 1.8ml/min

Length 30m

Inner diameter .25mm

Film thickness .25μm

Carrier gas He

Temperature ramps

Number of ramps 3

GC initial temperature 32°C

GC initial temperature hold time .25min

GC first temperature ramp rate 20°C/min

GC second temperature 60°C

GC second temperature hold time 0.00min

GC second temperature ramp rate 50°C/min

GC third temperature 150°C

GC third temperature hold time 0.00min

GC third temperature ramp rate 70°C/min

GC final temperature 280°C

GC final temperature hold time 2 min

Mass Spectrometer detectors TOF (Leco)

Scan mass range 29-400

Data rate 20Hz

Ionisation -70eV

Chickpea Roasted Porridge 2022

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Faith Zillinger

Michigan State University

Department of Food Science and Human Nutrition

Sample in glass vial

20ml

Solid-Phase Microextraction (SPME)

Sample details

Title Chickpea Roasted Porridge 2022

Project Pulse Flours

Citation https://doi.org/10.1111/1750-3841.70608

Collection method Sample in glass vial

Collection volume (of the vial) 20ml

Did not weight No

Mass of object sample 5g

Sample storage before sampling? No

Material state Fresh, Crushed

Suppressing enzyme-driven changes No

Increase headspace sensitivity (“salting out”) Yes

Salts Sodium chloride

Sampling method

Sampling method Solid-Phase Microextraction (SPME)

Robotic automation Yes

What platform? Gerstel MPS

Sorbent type DVB/CAR/PDMS

Sorbent phase thickness 30um

Headspace equilibrium temperature 50°C

Headspace equilibrium time 30min

Extraction mode Yes

Extraction time 30min

Extraction temperature 50°C

Desorption time 0.3min

Desorption temperature 200°C

Vortex No

GC-MS

Focusing trap Cooled Injection System

CIS low temperature -196°C

Trap split {Empty}

Column type HP-5

Column constant flow 1.8ml/min

Length 30m

Inner diameter .25mm

Film thickness .25μm

Carrier gas He

Temperature ramps

Number of ramps 3

GC initial temperature 32°C

GC initial temperature hold time .25min

GC first temperature ramp rate 20°C/min

GC second temperature 60°C

GC second temperature hold time 0.00min

GC second temperature ramp rate 50°C/min

GC third temperature 150°C

GC third temperature hold time 0.00min

GC third temperature ramp rate 70°C/min

GC final temperature 280°C

GC final temperature hold time 2 min

Mass Spectrometer detectors TOF (Leco)

Scan mass range 29-400

Data rate 20Hz

Ionisation -70eV

Chickpea Boiled Pulse 2022

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Faith Zillinger

Michigan State University

Department of Food Science and Human Nutrition

Sample in glass vial

20ml

Solid-Phase Microextraction (SPME)

Sample details

Title Chickpea Boiled Pulse 2022

Project Pulse Flours

Citation https://doi.org/10.1111/1750-3841.70608

Collection method Sample in glass vial

Collection volume (of the vial) 20ml

Did not weight No

Mass of object sample 5g

Sample storage before sampling? No

Material state Fresh, Crushed

Suppressing enzyme-driven changes No

Increase headspace sensitivity (“salting out”) No

Sampling method

Sampling method Solid-Phase Microextraction (SPME)

Robotic automation Yes

What platform? Gerstel MPS

Sorbent type DVB/CAR/PDMS

Sorbent phase thickness 30um

Headspace equilibrium temperature 50°C

Headspace equilibrium time 30min

Extraction mode Yes

Extraction time 30min

Extraction temperature 50°C

Desorption time 0.3min

Desorption temperature 200°C

Vortex No

GC-MS

Focusing trap Cooled Injection System

CIS low temperature -196°C

Trap split {Empty}

Column type HP-5

Column constant flow 1.8ml/min

Length 30m

Inner diameter .25mm

Film thickness .25μm

Carrier gas He

Temperature ramps

Number of ramps 3

GC initial temperature 32°C

GC initial temperature hold time .25min

GC first temperature ramp rate 20°C/min

GC second temperature 60°C

GC second temperature hold time 0.00min

GC second temperature ramp rate 50°C/min

GC third temperature 150°C

GC third temperature hold time 0.00min

GC third temperature ramp rate 70°C/min

GC final temperature 280°C

GC final temperature hold time 2 min

Mass Spectrometer detectors TOF (Leco)

Scan mass range 29-400

Data rate 20Hz

Ionisation -70eV

Chickpea Roasted Flour 2022

Download

view

Faith Zillinger

Michigan State University

Department of Food Science and Human Nutrition

Sample in glass vial

20ml

Solid-Phase Microextraction (SPME)

Sample details

Title Chickpea Roasted Flour 2022

Project Pulse Flours

Citation https://doi.org/10.1111/1750-3841.70608

Collection method Sample in glass vial

Collection volume (of the vial) 20ml

Did not weight No

Mass of object sample 2g

Sample storage before sampling? Yes

Sample storage temperature before sampling 2°C

Sample storage time before sampling 13140Hours

Material state Dried

Sampling method

Sampling method Solid-Phase Microextraction (SPME)

Robotic automation Yes

What platform? Gerstel MPS

Sorbent type DVB/CAR/PDMS

Sorbent phase thickness 30um

Headspace equilibrium temperature 50°C

Headspace equilibrium time 30min

Extraction mode Yes

Extraction time 30min

Extraction temperature 50°C

Desorption time 0.3min

Desorption temperature 200°C

Vortex No

GC-MS

Focusing trap Cooled Injection System

CIS low temperature -196°C

Trap split {Empty}

Column type HP-5

Column constant flow 1.8ml/min

Length 30m

Inner diameter .25mm

Film thickness .25μm

Carrier gas He

Temperature ramps

Number of ramps 3

GC initial temperature 32°C

GC initial temperature hold time .25min

GC first temperature ramp rate 20°C/min

GC second temperature 60°C

GC second temperature hold time 0.00min

GC second temperature ramp rate 50°C/min

GC third temperature 150°C

GC third temperature hold time 0.00min

GC third temperature ramp rate 70°C/min

GC final temperature 280°C

GC final temperature hold time 2 min

Mass Spectrometer detectors TOF (Leco)

Scan mass range 29-400

Data rate 20Hz

Ionisation -70eV

Alfalfa Blossoms Honey Bottle 2

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Faith Zillinger

Michigan State University

Department of Food Science and Human Nutrition

Sample in glass vial

40ml

Solid-Phase Microextraction (SPME)

Sample details

Title Alfalfa Blossoms Honey Bottle 2

Project Floral Honey

Date of collection 2024-02-18

Citation https://doi.org/10.1111/1750-3841.17461

Collection method Sample in glass vial

Collection volume (of the vial) 40ml

Did not weight No

Mass of object sample 8g

Sample storage before sampling? No

Material state Fresh

Sampling method

Sampling method Solid-Phase Microextraction (SPME)

Robotic automation No

Sorbent type DVB/PDMS

Sorbent phase thickness 65um

Headspace equilibrium temperature 40°C

Headspace equilibrium time 10min

Extraction mode Yes

Extraction time 10min

Extraction temperature 35°C

Desorption time .5min

Desorption temperature 200°C

Vortex Yes

Vortex speed 1000rpm

GC-MS

Focusing trap Cooled Injection System

CIS low temperature -196°C

Trap split {Empty}

Column type HP-5

Column constant flow 1.5ml/min

Length 60m

Inner diameter .25mm

Film thickness .25μm

Carrier gas He

Temperature ramps

Number of ramps 1

GC initial temperature 40°C

GC initial temperature hold time .5min

GC first temperature ramp rate 43°C/min

GC final temperature 280°C

Mass Spectrometer detectors TOF (Leco)

Scan mass range 29-400

Data rate 20Hz

Ionisation -70eV

Alfalfa Blossoms Honey Bottle 1

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Faith Zillinger

Michigan State University

Department of Food Science and Human Nutrition

Sample in glass vial

40ml

Solid-Phase Microextraction (SPME)

Sample details

Title Alfalfa Blossoms Honey Bottle 1

Project Floral Honey

Date of collection 2024-02-18

Citation https://doi.org/10.1111/1750-3841.17461

Collection method Sample in glass vial

Collection volume (of the vial) 40ml

Did not weight No

Mass of object sample 8g

Sample storage before sampling? No

Material state Fresh

Sampling method

Sampling method Solid-Phase Microextraction (SPME)

Robotic automation No

Sorbent type DVB/PDMS

Sorbent phase thickness 65um

Headspace equilibrium temperature 40°C

Headspace equilibrium time 10min

Extraction mode Yes

Extraction time 10min

Extraction temperature 35°C

Desorption time .5min

Desorption temperature 200°C

Vortex Yes

Vortex speed 1000rpm

GC-MS

Focusing trap Cooled Injection System

CIS low temperature -196°C

Trap split {Empty}

Column type HP-5

Column constant flow 1.5ml/min

Length 60m

Inner diameter .25mm

Film thickness .25μm

Carrier gas He

Temperature ramps

Number of ramps 1

GC initial temperature 40°C

GC initial temperature hold time .5min

GC first temperature ramp rate 43°C/min

GC final temperature 280°C

Mass Spectrometer detectors TOF (Leco)

Scan mass range 29-400

Data rate 20Hz

Ionisation -70eV

Orange Blossoms Honey Bottle 2

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Faith Zillinger

Michigan State University

Department of Food Science and Human Nutrition

Sample in glass vial

40ml

Solid-Phase Microextraction (SPME)

Sample details

Title Orange Blossoms Honey Bottle 2

Project Floral Honey

Date of collection 2024-02-18

Citation https://doi.org/10.1111/1750-3841.17461

Collection method Sample in glass vial

Collection volume (of the vial) 40ml

Did not weight No

Mass of object sample 8g

Sample storage before sampling? No

Material state Fresh

Sampling method

Sampling method Solid-Phase Microextraction (SPME)

Robotic automation No

Sorbent type DVB/PDMS

Sorbent phase thickness 65um

Headspace equilibrium temperature 40°C

Headspace equilibrium time 10min

Extraction mode Yes

Extraction time 10min

Extraction temperature 35°C

Desorption time .5min

Desorption temperature 200°C

Vortex Yes

Vortex speed 1000rpm

GC-MS

Focusing trap Cooled Injection System

CIS low temperature -196°C

Trap split {Empty}

Column type HP-5

Column constant flow 1.5ml/min

Length 60m

Inner diameter .25mm

Film thickness .25μm

Carrier gas He

Temperature ramps

Number of ramps 1

GC initial temperature 40°C

GC initial temperature hold time .5min

GC first temperature ramp rate 43°C/min

GC final temperature 280°C

Mass Spectrometer detectors TOF (Leco)

Scan mass range 29-400

Data rate 20Hz

Ionisation -70eV

Orange Blossoms Honey Bottle 1

Download

view

Faith Zillinger

Michigan State University

Department of Food Science and Human Nutrition

Sample in glass vial

40ml

Solid-Phase Microextraction (SPME)

Sample details

Title Orange Blossoms Honey Bottle 1

Project Floral Honey

Date of collection 2024-02-18

Citation https://doi.org/10.1111/1750-3841.17461

Collection method Sample in glass vial

Collection volume (of the vial) 40ml

Did not weight No

Mass of object sample 8g

Sample storage before sampling? No

Material state Fresh

Sampling method

Sampling method Solid-Phase Microextraction (SPME)

Robotic automation No

Sorbent type DVB/PDMS

Sorbent phase thickness 65um

Headspace equilibrium temperature 40°C

Headspace equilibrium time 10min

Extraction mode Yes

Extraction time 10min

Extraction temperature 35°C

Desorption time .5min

Desorption temperature 200°C

Vortex Yes

Vortex speed 1000rpm

GC-MS

Focusing trap Cooled Injection System

CIS low temperature -196°C

Trap split {Empty}

Column type HP-5

Column constant flow 1.5ml/min

Length 60m

Inner diameter .25mm

Film thickness .25μm

Carrier gas He

Temperature ramps

Number of ramps 1

GC initial temperature 40°C

GC initial temperature hold time .5min

GC first temperature ramp rate 43°C/min

GC final temperature 280°C

Mass Spectrometer detectors TOF (Leco)

Scan mass range 29-400

Data rate 20Hz

Ionisation -70eV